DIETHYLENE GLYCOL BIS(2-CHLOROETHYL) ETHER

Mass

MS-NW-6661          
diethylene glycol bis(2-chloroethyl) ether
C8H16Cl2O3          (Mass of molecular ion:    230)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       3.2
      19.0       1.1
      26.0       1.6
      27.0      29.9
      28.0       8.2
      29.0       5.1
      31.0       6.3
      36.0       1.0
      43.0      16.9
      44.0       4.9
      45.0      56.6
      46.0       1.4
      49.0       1.8
      51.0       3.3
      57.0       1.5
      58.0       1.4
      59.0      16.4
      62.0       2.8
      63.0     100.0
      64.0       3.3
      65.0      30.7
      70.0       1.5
      71.0       1.2
      72.0       3.1
      73.0       8.0
      87.0       3.4
      93.0       6.2
      95.0       2.2
     101.0       2.9
     103.0       1.0
     105.0       1.1
     106.0      17.7
     107.0      51.1
     108.0       8.0
     109.0      16.3
     115.0       1.5
     137.0      16.5
     138.0       1.1
     139.0       5.8
     151.0       1.9

Assign. Shift(ppm) A 3.78 B 3.68 C 3.62

     Hz     ppm     Int.

    345.25   3.855     27
    342.06   3.820     50
    340.38   3.801     23
    340.06   3.798     23
    337.00   3.763    149
    333.31   3.722    186
    332.69   3.715    198
    329.50   3.680   1000
    325.69   3.637    170
    320.63   3.581     60
    317.44   3.545     34