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MassMS-NW-4361 2-(2-chloroethoxy)ethanol C4H9ClO2 (Mass of molecular ion: 124)
Source Temperature: 230 °C Sample Temperature: 170 °C Reservoir, 75 eV
14.0 1.3 15.0 5.1 18.0 1.0 19.0 4.3 26.0 4.2 27.0 53.1 28.0 11.1 29.0 15.5 30.0 2.1 31.0 39.5 36.0 1.4 42.0 3.0 43.0 14.6 44.0 23.8 45.0 100.0 46.0 2.3 49.0 3.3 51.0 1.1 57.0 2.3 58.0 4.6 61.0 2.3 62.0 2.4 63.0 95.2 64.0 2.9 65.0 33.8 75.0 53.9 76.0 2.1 88.0 3.7 93.0 82.8 94.0 3.9 95.0 25.5 96.0 1.2
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C4 H9 Cl O2 0.041 g : 0.5 ml CDCl3 2-(2-chloroethoxy)ethanol 
Assign. Shift(ppm)
A 3.97 to 3.44 B 3.57
Hz ppm Int.345.63 3.860 78 342.38 3.823 180 341.56 3.814 119 339.50 3.791 163 337.69 3.771 366 337.31 3.767 375 336.81 3.761 404 336.31 3.756 387 335.38 3.745 299 334.19 3.732 706 333.56 3.725 720 331.56 3.703 995 331.00 3.696 941 327.88 3.662 736 327.38 3.656 750 325.06 3.630 297 324.06 3.619 267 322.81 3.605 293 321.13 3.586 223 319.88 3.572 1000 317.94 3.551 149 314.50 3.512 39 314.00 3.507 38 311.06 3.474 33
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1H NMR 399.65 MHz C4 H9 Cl O2 0.05 ml : 0.5 ml CDCl3 2-(2-chloroethoxy)ethanol Assign. Shift(ppm)
A 3.88 B 3.77 C 3.75 D 3.670 E 3.626
Hz ppm Int.1551.03 3.881 1000 1521.12 3.807 31 1520.51 3.805 33 1513.18 3.787 504 1512.33 3.785 486 1507.69 3.773 894 1507.20 3.772 912 1506.23 3.769 593 1505.74 3.768 386 1503.78 3.763 544 1501.83 3.758 840 1501.22 3.757 794 1499.39 3.752 649 1497.92 3.749 441 1496.09 3.744 241 1494.38 3.740 679 1483.64 3.713 39 1482.91 3.711 39 1481.93 3.709 39 1475.95 3.694 45 1471.92 3.684 756 1471.31 3.682 721 1467.41 3.672 383 1466.80 3.671 560 1465.82 3.668 892 1465.33 3.667 751 1462.89 3.661 81 1460.69 3.655 451 1459.96 3.654 436 1453.61 3.638 792 1451.90 3.633 241 1450.07 3.629 445 1448.73 3.625 669 1446.53 3.620 208 1444.21 3.614 520 1439.45 3.602 48
in CDCl3
liquid film
4880 A,200 M,liquid
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