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626-43-7

3,5-Dichloroaniline

Product Name 3,5-Dichloroaniline

CAS626-43-7

MFC6H5Cl2N

MW162.02

More

  • 626-43-7_ms
    Mass

    MS-NW-1615          
    3,5-dichloroaniline
    C6H5Cl2N            (Mass of molecular ion:    161)
    

       Source Temperature: 240 °C
       Sample Temperature: 180 °C
       Reservoir, 75 eV
    

          28.0       2.7
          37.0       2.5
          38.0       3.0
          39.0       3.0
          41.0       2.8
          44.5       4.2
          45.5       1.3
          49.0       1.0
          50.0       1.4
          52.0       3.6
          61.0       3.4
          62.0       5.9
          62.5       4.9
          63.0      13.4
          63.5       1.5
          64.0       3.2
          65.0       2.2
          73.0       4.6
          74.0       1.7
          75.0       1.7
          80.5       4.5
          81.5       2.9
          88.0       1.0
          89.0       2.2
          90.0      17.1
          91.0       4.5
          97.0       1.4
          98.0       2.3
          99.0      14.8
         100.0       1.7
         101.0       5.1
         124.0       1.0
         125.0       6.5
         126.0      12.2
         127.0       2.8
         128.0       3.8
         133.0       3.2
         134.0       4.3
         135.0       2.4
         136.0       2.6
         160.0       1.0
         161.0     100.0
         162.0       7.5
         163.0      64.0
         164.0       4.6
         165.0      10.2
    

90 MHz in CDCl3

  • 626-43-7_1hnmr

    1H NMR 89.56 MHz
    C6 H5 Cl2 N 0.044 g : 0.5 ml CDCl3
    3,5-dichloroaniline
    ChemicalStructure
        Assign.     Shift(ppm)
    A 6.711 B 6.519 C 3.8

         Hz     ppm     Int.
    

        603.06   6.734    190
        601.25   6.714    367
        599.56   6.695    297
        584.75   6.530   1000
        583.00   6.510    817
        581.44   6.493     42
        338.44   3.779     43
    

in CDCl3

CCl4 solution

KBr disc

nujol mull

OXIDATION WITH PERBENZOIC ACID