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MassMS-NW-1615 3,5-dichloroaniline C6H5Cl2N (Mass of molecular ion: 161)
Source Temperature: 240 °C Sample Temperature: 180 °C Reservoir, 75 eV
28.0 2.7 37.0 2.5 38.0 3.0 39.0 3.0 41.0 2.8 44.5 4.2 45.5 1.3 49.0 1.0 50.0 1.4 52.0 3.6 61.0 3.4 62.0 5.9 62.5 4.9 63.0 13.4 63.5 1.5 64.0 3.2 65.0 2.2 73.0 4.6 74.0 1.7 75.0 1.7 80.5 4.5 81.5 2.9 88.0 1.0 89.0 2.2 90.0 17.1 91.0 4.5 97.0 1.4 98.0 2.3 99.0 14.8 100.0 1.7 101.0 5.1 124.0 1.0 125.0 6.5 126.0 12.2 127.0 2.8 128.0 3.8 133.0 3.2 134.0 4.3 135.0 2.4 136.0 2.6 160.0 1.0 161.0 100.0 162.0 7.5 163.0 64.0 164.0 4.6 165.0 10.2
90 MHz in CDCl3
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1H NMR 89.56 MHz C6 H5 Cl2 N 0.044 g : 0.5 ml CDCl3 3,5-dichloroaniline 
Assign. Shift(ppm)
A 6.711 B 6.519 C 3.8
Hz ppm Int.603.06 6.734 190 601.25 6.714 367 599.56 6.695 297 584.75 6.530 1000 583.00 6.510 817 581.44 6.493 42 338.44 3.779 43
in CDCl3
CCl4 solution
KBr disc
nujol mull
OXIDATION WITH PERBENZOIC ACID
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