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MassMS-NW-9443 2,6-dimethoxypyridine C7H9NO2 (Mass of molecular ion: 139)
Source Temperature: 240 °C Sample Temperature: 160 °C Reservoir, 75 eV
15.0 4.4 26.0 2.1 27.0 2.5 28.0 2.4 29.0 1.2 37.0 2.6 38.0 10.7 39.0 25.3 40.0 2.1 41.0 3.1 42.0 3.1 50.0 1.8 51.0 1.9 52.0 4.3 53.0 5.4 54.0 3.8 55.0 5.9 64.0 5.8 65.0 10.2 66.0 16.3 67.0 2.5 68.0 3.6 69.5 1.0 70.0 2.2 77.0 1.4 78.0 7.3 79.0 4.5 80.0 14.5 81.0 5.2 82.0 1.4 91.0 5.3 92.0 1.6 93.0 13.1 94.0 21.8 95.0 4.5 96.0 7.5 106.0 3.2 107.0 1.1 108.0 14.2 109.0 38.3 110.0 28.4 111.0 2.0 120.0 2.7 121.0 6.1 122.0 1.2 123.0 1.4 124.0 10.3 138.0 100.0 139.0 98.3 140.0 8.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H9 N O2 0.05 ml : 0.5 ml CDCl3 2,6-dimethoxypyridine 
Assign. Shift(ppm)
A 7.445 B 6.277 C 3.891
Hz ppm Int.2983.64 7.466 185 2975.83 7.447 312 2967.90 7.427 195 2512.57 6.287 532 2504.76 6.268 516 1626.83 4.071 28 1555.30 3.892 1000 1481.45 3.707 27
in CDCl3
liquid film
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