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MS-NW-5426 tripentylamine C15H33N (Mass of molecular ion: 227)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 1.3 27.0 3.1 28.0 1.1 29.0 6.8 30.0 5.4 39.0 1.5 41.0 9.1 42.0 5.6 43.0 19.8 44.0 9.1 55.0 2.8 56.0 2.0 57.0 2.3 58.0 5.4 69.0 1.7 70.0 1.8 71.0 1.5 84.0 5.8 98.0 2.0 100.0 3.6 112.0 3.7 114.0 24.9 115.0 2.2 156.0 1.0 168.0 2.3 170.0 100.0 171.0 12.6 196.0 3.1 226.0 1.1 227.0 3.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C15 H33 N 0.04 ml : 0.5 ml CDCl3 tripentylamine Assign. Shift(ppm)
A 2.38 B 1.66 to 1.06 C 0.90
Hz ppm Int.
221.75 2.476 134 219.00 2.446 92 217.44 2.428 108 214.81 2.399 242 212.88 2.377 186 209.63 2.341 82 206.81 2.310 277 142.19 1.588 43 139.13 1.554 34 138.75 1.550 36 135.75 1.516 103 134.06 1.497 94 132.56 1.481 87 130.06 1.453 162 128.75 1.438 141 126.94 1.418 180 124.75 1.393 215 119.88 1.339 368 118.13 1.320 459 115.81 1.294 610 110.56 1.235 227 109.19 1.220 203 105.44 1.178 124 102.81 1.148 62 102.63 1.146 62 100.94 1.128 45 100.50 1.123 45 99.19 1.108 38 98.75 1.103 39 98.25 1.098 39 97.56 1.090 40 97.31 1.087 40 96.38 1.077 34 95.63 1.068 34 95.19 1.063 32 92.69 1.035 42 92.56 1.034 42 91.13 1.018 34 90.25 1.008 36 85.44 0.954 253 84.13 0.940 214 82.38 0.920 198 79.94 0.893 1000 73.75 0.824 185 72.69 0.812 183 69.94 0.781 66
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