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MassMS-NW-4744 3'-hydroxyacetanilide C8H9NO2 (Mass of molecular ion: 151)
Source Temperature: 160 °C Sample Temperature: 130 °C Direct, 75 eV
15.0 1.8 18.0 1.0 27.0 2.1 28.0 1.3 39.0 3.8 40.0 1.0 41.0 1.0 42.0 1.5 43.0 21.9 51.0 1.6 52.0 2.6 53.0 4.6 54.0 1.1 63.0 1.6 64.0 1.4 65.0 2.4 68.0 2.4 80.0 10.5 81.0 7.9 82.0 2.3 108.0 2.2 109.0 100.0 110.0 7.6 122.0 1.7 151.0 45.7 152.0 4.7
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H9 N O2 0.050 g : 0.5 ml CDCl3 3'-hydroxyacetanilide 
Assign. Shift(ppm)
A 9.77 B 9.33 C 7.203 D 7.04 E 6.94 F 6.442 G 2.025
Hz ppm Int.875.17 9.772 71 835.18 9.326 354 647.24 7.227 71 645.19 7.204 116 643.36 7.184 77 641.09 7.159 47 633.25 7.071 115 625.49 6.985 185 623.51 6.962 153 621.90 6.944 88 617.36 6.894 34 615.53 6.873 40 582.28 6.502 63 580.37 6.481 74 580.00 6.477 77 578.25 6.457 55 575.02 6.421 52 573.12 6.400 55 572.46 6.392 58 570.78 6.374 44 181.42 2.026 1000
KBr disc
nujol mull
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