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N,N-Dibenzylhydroxylamine

Product Name N,N-Dibenzylhydroxylamine

CAS621-07-8

MFC14H15NO

MW213.27

¹³CNMR

Mass

MS-IW-0794          
N,N-dibenzylhydroxylamine
C14H15NO            (Mass of molecular ion:    213)

   Source Temperature: 130 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      18.0       2.3
      39.0       2.0
      51.0       2.1
      63.0       1.4
      65.0       9.7
      77.0       2.8
      89.0       2.6
      90.0       1.8
      91.0     100.0
      92.0      18.6
      93.0       1.1
     104.0       1.9
     105.0       1.8
     106.0      13.8
     107.0       1.2
     117.0       2.3
     118.0       2.0
     120.0       1.6
     122.0       2.2
     168.0       1.0
     181.0       1.2
     194.0       7.2
     195.0       9.5
     196.0       3.8
     197.0       3.4
     211.0       2.1
     213.0      18.5
     214.0       3.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₁₅ N O	0.033 g : 0.5 ml CDCl₃
N,N-dibenzylhydroxylamine

    Assign.     Shift(ppm)

      A          7.30 to 7.25
      B             7.03
      C             3.631

     Hz     ppm     Int.

   2925.17   7.320    139
   2923.95   7.317    197
   2922.36   7.313    118
   2917.97   7.302    366
   2916.87   7.299    505
   2915.53   7.296    433
   2912.35   7.288    290
   2909.91   7.282    786
   2903.32   7.265   1000
   2900.02   7.257    478
   2898.80   7.254    431
   2896.61   7.248    505
   2894.78   7.244    337
   2891.72   7.236    365
   2888.55   7.228    117
   2886.72   7.224    167
   2885.01   7.219    123
   2883.30   7.215     72
   2808.84   7.029    287
   1451.29   3.632    814

in CDCl3

KBr disc

nujol mull

4880 A,200 M,liquid

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