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MS-NW-8751 2,2-dichlorovinyl dimethyl phosphate C4H7Cl2O4P (Mass of molecular ion: 220)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
15.0 13.0 28.0 1.1 29.0 2.0 31.0 2.7 47.0 6.3 48.0 1.6 49.0 1.2 50.0 1.0 60.0 1.5 76.0 2.8 78.0 1.1 79.0 17.6 83.0 2.3 85.0 1.4 93.0 2.5 95.0 1.7 97.0 2.2 109.0 100.0 110.0 3.1 111.0 1.3 113.0 2.3 145.0 6.2 147.0 2.0 185.0 18.3 187.0 6.0 220.0 4.0 222.0 2.6
in CDCl3
90 MHz in CDCl3
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1H NMR 89.56 MHz C4 H7 Cl2 O4 P 0.05 ml : 0.5 ml CDCl3 2,2-dichlorovinyl dimethyl phosphate Assign. Shift(ppm)
A 6.998 B 3.868 J(P-31,A)=5.2HZ. J(P-31,B)=11.4HZ.
Hz ppm Int.
629.38 7.028 208 624.13 6.969 210 352.13 3.932 1000 349.50 3.903 25 348.56 3.892 23 343.88 3.840 27 340.75 3.805 990 338.19 3.777 23
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