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MassMS-NW-0204 m-iodobenzoic acid C7H5IO2 (Mass of molecular ion: 248)
Source Temperature: 190 °C Sample Temperature: 0 °C Direct, 75 eV
37.0 1.7 38.0 2.2 39.0 6.2 45.0 1.9 49.0 1.7 50.0 18.2 51.0 6.1 53.0 1.6 63.0 1.4 64.0 1.4 65.0 30.0 66.0 1.7 73.0 2.2 74.0 10.6 75.0 10.6 76.0 19.5 77.0 2.5 92.0 1.9 93.0 3.2 103.0 2.3 104.0 1.5 115.5 1.5 121.0 26.7 122.0 2.2 127.0 4.8 203.0 8.3 231.0 11.5 232.0 1.0 248.0 100.0 249.0 7.9
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C7 H5 I O2 0.039 g : 0.5 ml DMSO-d6 m-iodobenzoic acid 
Assign. Shift(ppm)
A 13.3 B 8.255 C *1 8.000 D *1 7.967 E 7.333
Hz ppm Int.5321.80 13.317 41 3301.21 8.261 598 3299.50 8.256 1000 3297.79 8.252 577 3202.70 8.014 342 3201.63 8.012 447 3200.13 8.008 355 3194.79 7.994 373 3193.72 7.992 477 3192.23 7.988 394 3189.45 7.981 380 3188.17 7.978 498 3187.10 7.975 327 3181.76 7.962 391 3180.47 7.959 531 3179.41 7.956 318 2941.79 7.361 32 2938.37 7.353 495 2930.46 7.333 934 2926.83 7.324 36 2926.40 7.323 34 2925.98 7.322 34 2922.77 7.314 437
KBr disc
nujol mull
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