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N,N-Diethylformamide

Product Name N,N-Diethylformamide

CAS617-84-5

MFC5H11NO

MW101.15

¹³CNMR

Mass

MS-NW-1011          
N,N-diethylformamide
C5H11NO             (Mass of molecular ion:    101)

   Source Temperature: 260 °C
   Sample Temperature: 130 °C
   Reservoir, 75 eV

      15.0       5.7
      18.0       9.8
      26.0       3.5
      27.0      20.2
      28.0      18.3
      29.0      22.3
      30.0     100.0
      31.0       1.4
      40.0       1.7
      41.0       4.7
      42.0      12.5
      43.0       3.1
      44.0      41.7
      45.0       1.1
      54.0       1.0
      56.0       5.8
      57.0       1.6
      58.0      79.9
      59.0       2.8
      70.0       1.6
      72.0      15.5
      73.0       3.1
      86.0      36.8
      87.0       1.7
     100.0       1.6
     101.0      82.0
     102.0       4.9

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₅ H₁₁ N O	0.04 ml : 0.5 ml CDCl₃
N,N-diethylformamide

    Assign.     Shift(ppm)

      A             8.055
      B             3.342
      C             3.321
      D             1.202
      E             1.143

     Hz     ppm     Int.

    721.38   8.055    224
    313.06   3.496    100
    305.69   3.414    431
    298.50   3.333    678
    291.31   3.253    453
    284.06   3.172    116
    114.50   1.279    456
    109.00   1.218    411
    107.44   1.200   1000
    103.81   1.160     38
    101.81   1.137    775
    100.19   1.119    419
     94.63   1.057    331

in CDCl3

CCl4 solution

liquid film

4880 A,200 M,liquid

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