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MS-NW-1011 N,N-diethylformamide C5H11NO (Mass of molecular ion: 101)
Source Temperature: 260 °C Sample Temperature: 130 °C Reservoir, 75 eV
15.0 5.7 18.0 9.8 26.0 3.5 27.0 20.2 28.0 18.3 29.0 22.3 30.0 100.0 31.0 1.4 40.0 1.7 41.0 4.7 42.0 12.5 43.0 3.1 44.0 41.7 45.0 1.1 54.0 1.0 56.0 5.8 57.0 1.6 58.0 79.9 59.0 2.8 70.0 1.6 72.0 15.5 73.0 3.1 86.0 36.8 87.0 1.7 100.0 1.6 101.0 82.0 102.0 4.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H11 N O 0.04 ml : 0.5 ml CDCl3 N,N-diethylformamide Assign. Shift(ppm)
A 8.055 B 3.342 C 3.321 D 1.202 E 1.143
Hz ppm Int.
721.38 8.055 224 313.06 3.496 100 305.69 3.414 431 298.50 3.333 678 291.31 3.253 453 284.06 3.172 116 114.50 1.279 456 109.00 1.218 411 107.44 1.200 1000 103.81 1.160 38 101.81 1.137 775 100.19 1.119 419 94.63 1.057 331
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