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MS-NW-9732 2-chloro-p-toluidine C7H8ClN (Mass of molecular ion: 141)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
27.0 1.8 28.0 2.7 30.0 1.1 38.0 1.5 39.0 3.1 50.0 3.4 51.0 10.2 51.5 2.6 52.0 7.7 52.5 9.2 53.0 3.7 54.0 1.2 62.0 1.7 63.0 2.7 65.0 1.5 70.5 3.1 73.0 1.2 74.0 1.1 75.0 2.1 76.0 2.0 77.0 26.7 78.0 7.4 79.0 8.8 80.0 1.5 89.0 1.3 102.0 1.0 104.0 8.9 105.0 3.5 106.0 93.0 107.0 7.7 113.0 4.1 114.0 1.0 115.0 1.3 140.0 90.1 141.0 100.0 142.0 36.6 143.0 32.2 144.0 2.5
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H8 Cl N 0.05 ml : 0.5 ml CDCl3 2-chloro-p-toluidine Assign. Shift(ppm)
A 7.034 B 6.830 C 6.618 D 3.86 E 2.185
Hz ppm Int.
2812.13 7.037 195 2810.79 7.034 206 2735.60 6.845 94 2734.99 6.844 98 2733.64 6.841 96 2733.15 6.839 87 2727.54 6.825 116 2726.93 6.824 120 2725.59 6.820 120 2725.10 6.819 111 2648.56 6.628 295 2640.50 6.608 254 1541.87 3.859 62 1541.26 3.857 62 873.90 2.187 1000
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