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MS-NW-6430 o-methoxybenzyl alcohol C8H10O2 (Mass of molecular ion: 138)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 2.6 18.0 2.0 27.0 4.1 28.0 3.5 29.0 4.0 31.0 3.5 33.0 1.6 37.0 1.5 38.0 3.8 39.0 13.9 40.0 2.3 41.0 6.0 43.0 1.0 50.0 6.9 51.0 16.5 52.0 4.9 53.0 2.8 55.0 3.3 61.0 1.2 61.5 1.1 62.0 2.3 63.0 6.3 64.0 3.3 65.0 12.6 66.0 3.7 67.0 3.9 74.0 1.9 75.0 1.5 76.0 4.5 77.0 46.7 78.0 15.2 79.0 15.9 80.0 1.2 89.0 2.7 90.0 3.1 91.0 34.3 92.0 6.8 93.0 3.1 94.0 11.9 95.0 11.1 104.0 2.1 105.0 51.5 106.0 21.3 107.0 37.5 108.0 4.1 109.0 33.3 110.0 3.4 119.0 5.4 120.0 6.3 121.0 18.8 122.0 6.5 123.0 18.8 124.0 1.5 135.0 2.9 136.0 1.7 137.0 29.1 138.0 100.0 139.0 8.6
400 MHz in CDCl3
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1H NMR 399.65 MHz C8 H10 O2 0.05 ml : 0.5 ml CDCl3 o-methoxybenzyl alcohol Assign. Shift(ppm)
A 7.25 B 7.23 C 6.896 D 6.806 E 4.615 F 3.752 G 3.07 J(E,G)=3.7HZ
Hz ppm Int.
2900.88 7.259 67 2900.51 7.258 75 2899.78 7.256 73 2899.17 7.255 93 2898.68 7.254 93 2893.55 7.241 124 2893.19 7.240 116 2892.46 7.238 102 2891.85 7.236 144 2891.36 7.235 133 2886.11 7.222 99 2885.62 7.221 103 2884.28 7.218 73 2883.79 7.216 80 2878.05 7.202 79 2876.59 7.198 86 2876.22 7.197 74 2763.79 6.916 78 2762.82 6.914 86 2756.35 6.897 129 2755.37 6.895 144 2749.02 6.879 68 2747.92 6.876 74 2724.49 6.818 118 2723.75 6.816 118 2716.31 6.797 112 2715.58 6.795 111 1846.19 4.620 127 1842.53 4.611 138 1499.76 3.753 1000 1228.03 3.073 60
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