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MassMS-IW-3231 9-methylacridine C14H11N (Mass of molecular ion: 193)
Source Temperature: 110 °C Sample Temperature: 70 °C Direct, 75 eV
39.0 1.2 51.0 1.5 63.0 1.7 69.5 1.0 75.0 1.3 77.0 1.1 81.0 1.2 82.0 1.9 83.0 6.8 89.0 1.5 95.0 5.8 96.0 5.7 139.0 1.6 140.0 1.3 163.0 1.5 164.0 2.1 165.0 5.5 166.0 2.3 167.0 3.2 168.0 1.3 169.0 2.3 177.0 1.6 190.0 4.8 191.0 11.7 192.0 23.2 193.0 100.0 194.0 15.5 195.0 1.2
400 MHz in CDCl3
parameter in CDCl3
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1H NMR 399.65 MHz C14 H11 N 0.039 g : 0.5 ml CDCl3 9-methylacridine 
Assign. Shift(ppm)
A 8.196 B 8.158 C 7.723 D 7.490 E 3.017
Hz ppm Int.3280.40 8.209 202 3271.73 8.187 224 3265.87 8.172 171 3265.14 8.171 194 3264.53 8.169 202 3257.08 8.150 176 3256.35 8.149 206 3255.74 8.147 211 3255.13 8.145 176 3095.09 7.745 116 3093.75 7.742 118 3088.62 7.729 139 3087.16 7.725 155 3086.43 7.723 140 3085.08 7.720 115 3079.83 7.707 125 3078.49 7.703 125 3001.34 7.510 125 3000.12 7.507 129 2994.75 7.494 116 2993.53 7.491 134 2992.55 7.488 140 2991.33 7.485 127 2985.96 7.472 104 2984.74 7.469 105 1205.81 3.018 1000
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1H NMR 300 MHz C14 H11 N 0.7 M in CDCl3 9-methylacridine Parameter ppm Hz
D(A) 8.027 D(B) 7.398 D(C) 7.660 D(D) 8.163 J(A,B) 8.33 J(A,C) 1.36 J(A,D) 0.74 J(B,C) 6.62 J(B,D) 1.29 J(C,D) 8.77 D(E) 2.88 SCIACOVELLI,O. & VON PHILIPSBORN,W. ORG.MAGN.RESON. 3, 339 (1971)
Hz ppm Int.2454.46 8.182 101 2453.62 8.179 127 2453.23 8.177 128 2452.44 8.175 107 2445.70 8.152 114 2444.86 8.150 143 2444.47 8.148 143 2443.68 8.146 120 2413.43 8.045 106 2412.69 8.042 122 2412.10 8.040 124 2411.31 8.038 103 2405.12 8.017 115 2404.38 8.015 133 2403.79 8.013 137 2403.05 8.010 115 2306.38 7.688 88 2305.05 7.683 88 2299.79 7.666 107 2298.41 7.661 117 2297.67 7.659 98 2296.30 7.654 81 2291.03 7.637 94 2289.71 7.632 91 2227.28 7.424 104 2226.05 7.420 103 2220.69 7.402 93 2219.11 7.397 141 2217.73 7.392 99 2212.37 7.375 81 2211.09 7.370 79 864.00 2.880 1000
in CDCl3
KBr disc
nujol mull
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