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MassMS-NW-0148 8-methylquinoline C10H9N (Mass of molecular ion: 143)
Source Temperature: 220 °C Sample Temperature: 75 °C Reservoir, 75 eV
38.0 1.5 39.0 5.5 50.0 2.8 51.0 3.9 52.0 1.1 58.5 5.6 62.0 2.9 63.0 6.9 64.0 1.8 65.0 2.1 70.5 4.7 71.5 4.2 74.0 1.6 75.0 2.0 76.0 1.4 77.0 1.1 87.0 1.4 88.0 1.7 89.0 6.4 90.0 2.0 113.0 1.9 114.0 3.1 115.0 14.3 116.0 6.2 117.0 5.6 140.0 2.5 141.0 8.1 142.0 43.2 143.0 100.0 144.0 11.1
90 MHz in CDCl3
400 MHz in CDCl3
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1H NMR 89.56 MHz C10 H9 N 0.025 g : 0.5 ml CDCl3 8-methylquinoline 
Assign. Shift(ppm)
A 8.939 B 8.106 C 7.64 D 7.57 E 7.44 F 7.38 G 2.825 J(A,B)=1.8HZ. J(A,F)=4.2HZ. J(B,F)=8.3HZ.
Hz ppm Int.803.75 8.975 116 801.94 8.955 125 799.56 8.928 124 797.75 8.908 126 731.44 8.168 119 729.63 8.147 114 723.13 8.075 151 721.31 8.054 139 690.38 7.709 54 688.44 7.687 56 682.88 7.625 104 682.38 7.620 99 680.75 7.602 168 675.19 7.539 162 674.44 7.531 159 672.06 7.505 74 670.13 7.483 286 666.25 7.440 164 662.81 7.401 198 657.94 7.347 127 655.69 7.322 48 653.75 7.300 115 649.56 7.253 88 252.94 2.825 1000
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1H NMR 399.65 MHz C10 H9 N 0.025 g : 0.5 ml CDCl3 8-methylquinoline Assign. Shift(ppm)
A 8.949 B 8.120 C 7.653 D 7.560 E 7.432 F 7.386 G 2.826 J(A,B)=1.7HZ. J(A,F)=4.2HZ. J(B,F)=8.3HZ. J(C,E)=8.1HZ. J(D,E)=7.1HZ.
Hz ppm Int.3579.83 8.958 130 3578.13 8.954 142 3575.68 8.948 146 3573.85 8.943 151 3250.37 8.134 141 3248.66 8.129 151 3242.07 8.113 152 3240.36 8.108 159 3063.48 7.666 104 3062.99 7.665 104 3055.42 7.646 126 3054.81 7.644 126 3026.61 7.574 77 3025.51 7.571 98 3024.29 7.568 85 3023.32 7.565 43 3020.51 7.558 46 3019.53 7.556 106 3018.55 7.553 131 3017.33 7.550 106 3016.36 7.548 52 2977.17 7.450 161 2970.09 7.432 139 2969.12 7.430 156 2962.04 7.412 108 2957.76 7.401 181 2953.61 7.391 181 2949.58 7.381 173 2945.31 7.370 170 1129.64 2.827 1000
in CDCl3
liquid film
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