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MS-IW-3828 o-iodobenzoyl chloride C7H4ClIO (Mass of molecular ion: 266)
Source Temperature: 220 °C Sample Temperature: 150 °C Reservoir, 75 eV
49.0 1.0 50.0 10.0 73.0 1.1 74.0 5.2 75.0 6.8 76.0 20.2 77.0 1.7 104.0 2.7 111.0 2.0 115.5 3.4 127.0 2.8 203.0 24.3 204.0 1.7 231.0 100.0 232.0 7.8 266.0 13.3 267.0 1.0 268.0 4.4
400 MHz in CDCl3
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1H NMR 399.65 MHz C7 H4 Cl I O 0.040 g : 0.5 ml CDCl3 o-iodobenzoyl chloride Assign. Shift(ppm)
A 8.080 B 8.050 C 7.505 D 7.254
Hz ppm Int.
3234.50 8.094 739 3234.13 8.093 750 3232.79 8.090 805 3226.20 8.073 850 3224.85 8.070 870 3221.80 8.062 838 3220.95 8.060 960 3216.55 8.049 57 3214.23 8.043 865 3213.87 8.042 903 3213.01 8.040 1000 3206.79 8.024 31 3008.06 7.527 569 3006.84 7.524 579 3000.61 7.509 793 3000.12 7.507 723 2999.39 7.506 816 2998.90 7.504 653 2992.68 7.489 632 2991.46 7.486 641 2909.06 7.280 52 2907.47 7.276 659 2905.88 7.272 631 2900.02 7.257 753 2899.54 7.256 742 2898.44 7.253 715 2897.95 7.252 698 2894.41 7.243 45 2893.68 7.241 59 2892.09 7.237 554 2890.50 7.233 577
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