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MS-NW-4319 N,N-dimethylethylamine C4H11N (Mass of molecular ion: 73)
Source Temperature: 230 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 8.1 18.0 2.0 26.0 1.4 27.0 5.8 28.0 5.4 29.0 6.6 30.0 13.1 40.0 1.3 41.0 2.7 42.0 21.3 43.0 6.6 44.0 23.9 54.0 1.0 56.0 7.4 57.0 4.9 58.0 100.0 59.0 3.8 70.0 1.7 71.0 1.3 72.0 20.6 73.0 25.2 74.0 1.3
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C4 H11 N 0.05 ml : 0.5 ml CDCl3 N,N-dimethylethylamine Assign. Shift(ppm)
A 2.317 B 2.219 C 1.064
Hz ppm Int.
937.01 2.345 99 929.81 2.327 256 922.61 2.309 264 915.41 2.291 107 886.84 2.220 1000 432.50 1.083 310 425.29 1.065 520 418.09 1.047 311
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1H NMR 89.56 MHz C4 H11 N 0.02 ml : 0.5 ml CDCl3 N,N-dimethylethylamine Assign. Shift(ppm)
A 2.32 B 2.218 C 1.063
Hz ppm Int.
211.31 2.360 63 204.13 2.280 70 198.63 2.218 1000 196.00 2.189 28 102.00 1.139 83 95.13 1.063 186 94.69 1.058 127 87.75 0.980 62
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