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MS-NW-3224 N,N-dimethylallylamine C5H11N (Mass of molecular ion: 85)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 8.0 18.0 1.1 26.0 1.0 27.0 3.1 28.0 2.8 29.0 2.4 30.0 7.4 38.0 1.8 39.0 10.5 40.0 2.0 41.0 23.5 42.0 41.9 43.0 7.7 44.0 11.6 55.0 1.0 56.0 1.3 57.0 1.4 58.0 100.0 59.0 4.1 68.0 3.2 69.0 1.3 70.0 11.3 78.0 2.6 82.0 2.5 83.0 1.6 84.0 24.6 85.0 40.5 86.0 2.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C5 H11 N 0.04 ml : 0.5 ml CDCl3 N,N-dimethylallylamine Assign. Shift(ppm)
A 5.833 B 5.14 C 5.10 D 2.910 E 2.219 J(A,B)=17.3HZ. J(A,C)=9.7HZ. J(A,D)=6.4HZ. J(B,D)=J(C,D)=1.1HZ.
Hz ppm Int.
512.13 5.719 42 470.00 5.248 33 468.88 5.236 56 467.56 5.221 30 463.56 5.176 50 462.44 5.164 37 453.56 5.065 51 451.94 5.047 64 450.81 5.034 30 263.63 2.944 78 262.50 2.931 50 257.25 2.873 73 256.06 2.860 45 198.81 2.220 1000
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