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2-Bromoethyl ethyl ether

Product Name 2-Bromoethyl ethyl ether

CAS592-55-2

MFC4H9BrO

MW153.02

¹³CNMR

Mass

MS-NW-2560          
1-bromo-2-ethoxyethane
C4H9BrO             (Mass of molecular ion:    152)

   Source Temperature: 280 °C
   Sample Temperature: 170 °C
   Reservoir, 75 eV

      15.0       3.2
      26.0       2.9
      27.0      25.5
      28.0       5.7
      29.0      22.4
      31.0      50.0
      41.0       2.9
      43.0       5.6
      44.0       2.0
      45.0       6.8
      59.0     100.0
      60.0       3.2
      93.0       1.0
      95.0       1.1
     107.0      16.1
     109.0      15.7
     123.0       1.2
     125.0       1.0
     152.0       5.0
     154.0       5.0

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₄ H₉ Br O	0.05 ml : 0.5 ml CDCl₃
1-bromo-2-ethoxyethane

    Assign.     Shift(ppm)

      A             3.73
      B             3.55
      C             3.46
      D             1.224

     Hz     ppm     Int.

    342.94   3.830    133
    341.25   3.811    154
    337.38   3.768    161
    335.94   3.752    209
    335.19   3.743    566
    330.38   3.689    320
    329.38   3.678    468
    327.56   3.658    288
    322.19   3.598    525
    315.19   3.520    673
    311.06   3.474     27
    309.94   3.461    533
    309.19   3.453    251
    308.19   3.442    225
    307.75   3.437    219
    303.88   3.394    152
    302.13   3.374    135
    116.31   1.299    527
    109.38   1.222   1000
    102.31   1.143    452

in CDCl3

liquid film

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