Cbz-D-Phenylalaninol

Mass

MS-KW-0564          
N-benzyloxycarbonyl-D-phenylalaninol
C17H19NO3           (Mass of molecular ion:    271)

   Source Temperature: 160 °C
   Sample Temperature: 150 °C
   Direct, 75 eV

      15.0       3.2
      18.0       3.3
      27.0       3.5
      28.0       3.7
      29.0       2.3
      30.0       1.2
      31.0       1.4
      38.0       2.1
      39.0      10.4
      40.0       1.1
      41.0       2.7
      42.0      31.7
      43.0       5.9
      44.0       1.4
      50.0       6.4
      51.0      15.1
      52.0       4.3
      53.0       3.7
      53.5       1.2
      54.0       1.2
      58.0       6.9
      62.0       2.2
      63.0       6.2
      64.0       1.7
      65.0      16.6
      66.0       1.3
      74.0       2.1
      75.0       1.4
      76.0       1.5
      77.0      27.9
      78.0      10.0
      79.0      45.6
      80.0       4.5
      85.0       3.8
      86.0      71.5
      87.0       3.1
      89.0       5.8
      90.0       5.8
      91.0     100.0
      92.0      97.1
      93.0       7.3
     103.0       2.9
     104.0       1.9
     105.0       6.8
     106.0       2.1
     107.0      32.2
     108.0      39.7
     109.0       3.1
     115.0       2.7
     116.0       2.0
     117.0       1.7
     118.0       1.0
     133.0       1.4
     134.0       6.2
     150.0       3.7
     177.0       6.4
     178.0       1.1
     194.0       3.4

Assign. Shift(ppm) A 7.31 to 7.26 B 7.19 C 5.18 D 5.041 E 3.925 F *1 3.620 G *1 3.521 J 2.827 K 2.74

     Hz     ppm     Int.

   2936.65   7.346     96
   2934.09   7.340    138
   2928.23   7.325    298
   2926.88   7.322    269
   2924.93   7.317    258
   2921.03   7.307    775
   2919.19   7.302    521
   2917.61   7.298    418
   2913.21   7.287    650
   2904.42   7.265    506
   2896.98   7.247    331
   2891.61   7.233    197
   2885.87   7.219    216
   2878.79   7.201    278
   2872.93   7.187    309
   2866.34   7.170    212
   2072.76   5.185     77
   2063.60   5.162     63
   2015.26   5.041   1000
   2002.32   5.009     26
   1568.97   3.925     76
   1451.91   3.632     69
   1443.85   3.612    104
   1410.53   3.529     87
   1403.20   3.510     62
   1133.31   2.835    229
   1126.84   2.819    233
   1093.02   2.735     68