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58917-85-4

Cbz-D-Phenylalaninol

Product Name Cbz-D-Phenylalaninol

CAS58917-85-4

MFC17H19NO3

MW285.34

  • 58917-85-4_ms_1
    Mass

    MS-KW-0564          
    N-benzyloxycarbonyl-D-phenylalaninol
    C17H19NO3           (Mass of molecular ion:    271)
    

       Source Temperature: 160 °C
       Sample Temperature: 150 °C
       Direct, 75 eV
    

          15.0       3.2
          18.0       3.3
          27.0       3.5
          28.0       3.7
          29.0       2.3
          30.0       1.2
          31.0       1.4
          38.0       2.1
          39.0      10.4
          40.0       1.1
          41.0       2.7
          42.0      31.7
          43.0       5.9
          44.0       1.4
          50.0       6.4
          51.0      15.1
          52.0       4.3
          53.0       3.7
          53.5       1.2
          54.0       1.2
          58.0       6.9
          62.0       2.2
          63.0       6.2
          64.0       1.7
          65.0      16.6
          66.0       1.3
          74.0       2.1
          75.0       1.4
          76.0       1.5
          77.0      27.9
          78.0      10.0
          79.0      45.6
          80.0       4.5
          85.0       3.8
          86.0      71.5
          87.0       3.1
          89.0       5.8
          90.0       5.8
          91.0     100.0
          92.0      97.1
          93.0       7.3
         103.0       2.9
         104.0       1.9
         105.0       6.8
         106.0       2.1
         107.0      32.2
         108.0      39.7
         109.0       3.1
         115.0       2.7
         116.0       2.0
         117.0       1.7
         118.0       1.0
         133.0       1.4
         134.0       6.2
         150.0       3.7
         177.0       6.4
         178.0       1.1
         194.0       3.4
    

400 MHz in CDCl3

  • 58917-85-4_1hnmr_1

    1H NMR 399.65 MHz
    C17H19NO3 0.038 g : 0.5 ml CDCl3
    N-benzyloxycarbonyl-D-phenylalaninol
    ChemicalStructure
        Assign.     Shift(ppm)
    A 7.31 to 7.26 B 7.19 C 5.18 D 5.041 E 3.925 F *1 3.620 G *1 3.521 J 2.827 K 2.74

         Hz     ppm     Int.
    

       2936.65   7.346     96
       2934.09   7.340    138
       2928.23   7.325    298
       2926.88   7.322    269
       2924.93   7.317    258
       2921.03   7.307    775
       2919.19   7.302    521
       2917.61   7.298    418
       2913.21   7.287    650
       2904.42   7.265    506
       2896.98   7.247    331
       2891.61   7.233    197
       2885.87   7.219    216
       2878.79   7.201    278
       2872.93   7.187    309
       2866.34   7.170    212
       2072.76   5.185     77
       2063.60   5.162     63
       2015.26   5.041   1000
       2002.32   5.009     26
       1568.97   3.925     76
       1451.91   3.632     69
       1443.85   3.612    104
       1410.53   3.529     87
       1403.20   3.510     62
       1133.31   2.835    229
       1126.84   2.819    233
       1093.02   2.735     68
    

in CDCl3

  • 58917-85-4_13cnmr_1

KBr disk

  • 58917-85-4_ir1_2

Nujol

  • 58917-85-4_ir2_1