N,N''-BIS(2-HYDROXY-ALPHA-PHENYLBENZYLIDENE)ETHYLENEDIAMINE)

Mass

MS-IW-0026          
N,N'-bis(2-hydroxy-alpha-phenylbenzylidene)ethylenediamine
C28H24N2O2          (Mass of molecular ion:    420)

   Source Temperature: 210 °C
   Sample Temperature: 170 °C
   Direct, 75 eV

      39.0       2.0
      51.0       2.9
      63.0       1.4
      65.0       3.2
      76.0       1.6
      77.0       9.2
      78.0       1.9
      79.0       1.3
      91.0      22.8
      92.0       2.8
     102.0       2.2
     103.0       1.9
     104.0       7.1
     105.0       2.7
     107.0       9.9
     115.0       1.5
     116.0       4.0
     117.0       1.9
     118.0       1.0
     119.0       1.2
     120.0      10.2
     121.0       1.4
     127.0       1.4
     128.0       1.1
     130.0       2.8
     132.0       1.6
     143.0       1.2
     146.0       2.1
     151.0       2.4
     152.0       8.5
     153.0       3.8
     161.0       2.2
     165.0       3.5
     166.0       1.3
     167.0       2.5
     168.0       1.7
     178.0      12.5
     179.0       2.9
     180.0       4.6
     181.0      13.4
     182.0       4.6
     183.0       2.8
     184.0       2.3
     193.0       2.0
     194.0      21.8
     195.0       6.9
     196.0      39.5
     197.0      31.9
     198.0      29.7
     199.0       4.2
     206.0       2.6
     207.0       2.0
     208.0      23.7
     209.0       8.2
     210.0      33.5
     210.5       1.1
     211.0       6.2
     212.0       3.3
     220.0       1.6
     221.0       2.0
     222.0      37.9
     223.0     100.0
     224.0      30.9
     225.0       4.4
     236.0       1.3
     237.0       1.3
     238.0       1.9
     416.0       2.1
     420.0      65.1
     421.0      21.8
     422.0       3.9

Assign. Shift(ppm) A 15.2 B 7.48 C 7.47 D 7.253 E 7.137 F 6.972 G 6.765 J 6.627 K 3.619 CONFIRMED BY LAOCN PROGRAM

     Hz     ppm     Int.

   6081.45  15.217    212
   2995.42   7.496    102
   2993.93   7.492     78
   2991.36   7.485    326
   2989.65   7.481    347
   2986.66   7.474    553
   2984.53   7.468    638
   2981.96   7.462    106
   2981.32   7.460     87
   2980.25   7.458     72
   2907.60   7.276    101
   2905.89   7.272    105
   2900.33   7.258    125
   2899.27   7.255    162
   2898.84   7.254    160
   2897.56   7.251    143
   2892.21   7.237    119
   2890.29   7.233    120
   2858.67   7.153     60
   2856.74   7.149    270
   2855.67   7.146    196
   2854.39   7.143    174
   2853.32   7.140    232
   2852.47   7.138    285
   2850.55   7.133    116
   2849.26   7.130    304
   2847.13   7.125    256
   2843.71   7.116     38
   2790.93   6.984    217
   2790.07   6.982    222
   2782.59   6.963    193
   2781.74   6.961    187
   2709.09   6.779    151
   2707.38   6.775    156
   2700.97   6.759    214
   2699.47   6.755    198
   2656.09   6.647    134
   2655.02   6.644    147
   2649.04   6.629    166
   2647.97   6.626    194
   2647.12   6.624    144
   2641.14   6.609    110
   2639.85   6.606    109
   1446.43   3.620   1000