N,N''-BIS(2-HYDROXY-ALPHA-PHENYLBENZYLIDENE)ETHYLENEDIAMINE)
Product Name N,N''-BIS(2-HYDROXY-ALPHA-PHENYLBENZYLIDENE)ETHYLENEDIAMINE)
CAS58520-18-6
MFC28H24N2O2
MW420.5
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MassMS-IW-0026 N,N'-bis(2-hydroxy-alpha-phenylbenzylidene)ethylenediamine C28H24N2O2 (Mass of molecular ion: 420)
Source Temperature: 210 °C Sample Temperature: 170 °C Direct, 75 eV
39.0 2.0 51.0 2.9 63.0 1.4 65.0 3.2 76.0 1.6 77.0 9.2 78.0 1.9 79.0 1.3 91.0 22.8 92.0 2.8 102.0 2.2 103.0 1.9 104.0 7.1 105.0 2.7 107.0 9.9 115.0 1.5 116.0 4.0 117.0 1.9 118.0 1.0 119.0 1.2 120.0 10.2 121.0 1.4 127.0 1.4 128.0 1.1 130.0 2.8 132.0 1.6 143.0 1.2 146.0 2.1 151.0 2.4 152.0 8.5 153.0 3.8 161.0 2.2 165.0 3.5 166.0 1.3 167.0 2.5 168.0 1.7 178.0 12.5 179.0 2.9 180.0 4.6 181.0 13.4 182.0 4.6 183.0 2.8 184.0 2.3 193.0 2.0 194.0 21.8 195.0 6.9 196.0 39.5 197.0 31.9 198.0 29.7 199.0 4.2 206.0 2.6 207.0 2.0 208.0 23.7 209.0 8.2 210.0 33.5 210.5 1.1 211.0 6.2 212.0 3.3 220.0 1.6 221.0 2.0 222.0 37.9 223.0 100.0 224.0 30.9 225.0 4.4 236.0 1.3 237.0 1.3 238.0 1.9 416.0 2.1 420.0 65.1 421.0 21.8 422.0 3.9
400 MHz in CDCl3
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1H NMR 399.65 MHz C28 H24 N2 O2 0.030 g : 0.5 ml CDCl3 N,N'-bis(2-hydroxy-alpha-phenylbenzylidene)ethylenediamine 
Assign. Shift(ppm)
A 15.2 B 7.48 C 7.47 D 7.253 E 7.137 F 6.972 G 6.765 J 6.627 K 3.619 CONFIRMED BY LAOCN PROGRAM
Hz ppm Int.6081.45 15.217 212 2995.42 7.496 102 2993.93 7.492 78 2991.36 7.485 326 2989.65 7.481 347 2986.66 7.474 553 2984.53 7.468 638 2981.96 7.462 106 2981.32 7.460 87 2980.25 7.458 72 2907.60 7.276 101 2905.89 7.272 105 2900.33 7.258 125 2899.27 7.255 162 2898.84 7.254 160 2897.56 7.251 143 2892.21 7.237 119 2890.29 7.233 120 2858.67 7.153 60 2856.74 7.149 270 2855.67 7.146 196 2854.39 7.143 174 2853.32 7.140 232 2852.47 7.138 285 2850.55 7.133 116 2849.26 7.130 304 2847.13 7.125 256 2843.71 7.116 38 2790.93 6.984 217 2790.07 6.982 222 2782.59 6.963 193 2781.74 6.961 187 2709.09 6.779 151 2707.38 6.775 156 2700.97 6.759 214 2699.47 6.755 198 2656.09 6.647 134 2655.02 6.644 147 2649.04 6.629 166 2647.97 6.626 194 2647.12 6.624 144 2641.14 6.609 110 2639.85 6.606 109 1446.43 3.620 1000
in CDCl3
KBr disc
nujol mull
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