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MS-NW-8350 (1-bromoethyl)benzene C8H9Br (Mass of molecular ion: 184)
Source Temperature: 260 °C Sample Temperature: 140 °C Reservoir, 75 eV
27.0 3.5 38.0 1.0 39.0 4.0 50.0 4.0 51.0 10.6 52.0 3.2 62.0 1.1 63.0 2.8 65.0 1.1 74.0 1.5 75.0 1.1 76.0 1.4 77.0 14.2 78.0 8.1 79.0 14.3 80.0 1.0 89.0 1.3 91.0 1.7 102.0 1.7 103.0 11.9 104.0 13.6 105.0 100.0 106.0 9.4
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H9 Br 0.05 ml : 0.5 ml CDCl3 (1-bromoethyl)benzene Assign. Shift(ppm)
A 7.38 to 7.25 B 5.170 C 2.001
Hz ppm Int.
669.63 7.477 62 667.69 7.456 73 665.69 7.433 107 664.25 7.417 131 663.13 7.405 142 661.06 7.382 274 658.81 7.357 403 657.69 7.344 202 656.56 7.331 277 655.00 7.314 391 654.25 7.306 376 652.75 7.289 317 651.75 7.278 222 650.31 7.262 266 649.38 7.251 352 648.19 7.238 152 647.00 7.225 294 645.88 7.212 106 644.56 7.197 68 643.81 7.189 66 473.50 5.287 55 466.50 5.209 162 459.63 5.133 168 452.69 5.055 60 182.69 2.040 1000 175.75 1.963 950
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