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4-BROMO-2-METHYLANILINE

Product Name 4-BROMO-2-METHYLANILINE

CAS583-75-5

MFC7H8BrN

MW186.05

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  • Mass 

    MS-NW-6224          
4-bromo-o-toluidine
C7H8BrN             (Mass of molecular ion:    185)


       Source Temperature: 240 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV


          18.0       1.2
      26.0       1.1
      27.0       3.6
      28.0       5.2
      30.0       4.7
      37.0       1.9
      38.0       3.9
      39.0       6.9
      39.5       1.0
      40.0       1.4
      41.0       2.9
      42.0       2.1
      49.0       1.1
      50.0       6.9
      51.0      12.0
      51.5       2.7
      52.0      10.4
      52.5       8.6
      53.0      12.4
      54.0       3.2
      61.0       1.5
      62.0       2.9
      63.0       5.8
      64.0       1.9
      65.0       2.7
      66.0       1.9
      74.0       2.5
      75.0       2.6
      76.0       2.7
      77.0      22.2
      78.0      13.6
      79.0      17.9
      80.0       2.6
      89.0       7.1
      90.0       1.6
      91.0       1.1
      92.5       3.0
      93.5       2.9
     104.0      10.3
     105.0       9.2
     106.0      84.4
     107.0       7.2
     184.0      18.4
     185.0     100.0
     186.0      25.2
     187.0      96.5
     188.0       8.2

90 MHz in CDCl3


  • 1H NMR 89.56 MHz
    C7 H8 Br N 0.041 g : 0.5 ml CDCl3
    4-bromo-o-toluidine
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             7.16
      B             7.08
      C             6.521
      D             3.55
      E             2.119
  

         Hz     ppm     Int.


        640.94   7.157    366
    640.25   7.149    394
    639.56   7.142    253
    638.81   7.133    155
    633.63   7.075    131
    633.06   7.069    138
    631.25   7.049     87
    630.69   7.043     88
    588.31   6.569    148
    587.00   6.555    105
    581.00   6.488     60
    579.63   6.472    114
    317.50   3.546     60
    189.81   2.120   1000

in CDCl3



KBr disc



nujol mull





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