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MassMS-NW-1442 N-(2-naphthyl)acetamide C12H11NO (Mass of molecular ion: 185)
Source Temperature: 250 °C Sample Temperature: 170 °C Reservoir, 75 eV
14.0 1.0 15.0 1.7 17.0 2.6 18.0 11.9 39.0 2.3 43.0 13.5 44.0 3.2 50.0 1.4 51.0 1.8 62.0 1.6 63.0 3.6 65.0 1.8 74.0 1.1 75.0 1.6 76.0 1.0 77.0 1.2 88.0 1.3 89.0 3.4 113.0 1.6 114.0 2.9 115.0 24.7 116.0 7.5 117.0 1.1 126.0 1.3 127.0 2.0 140.0 2.0 141.0 1.4 142.0 2.8 143.0 100.0 144.0 12.3 145.0 1.0 185.0 41.6 186.0 6.0
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C12 H11 N O 0.020 g : 0.5 ml CDCl3 N-(2-naphthyl)acetamide 
Assign. Shift(ppm)
A 8.173 B 7.90 C 7.75 D 7.74 E 7.73 F 7.46 G *1 7.42 J *1 7.39 K 2.197 J(A,F)=1.8HZ.
Hz ppm Int.3267.21 8.176 133 3265.38 8.171 132 3154.17 7.893 51 3101.20 7.760 100 3095.70 7.747 150 3092.16 7.738 155 3087.16 7.725 149 3082.89 7.714 101 2984.62 7.469 99 2982.42 7.463 98 2975.71 7.446 96 2973.63 7.441 112 2967.41 7.426 93 2966.06 7.422 92 2959.72 7.406 96 2957.89 7.402 144 2956.18 7.397 99 2949.71 7.381 85 2948.49 7.378 81 2942.99 7.364 38 2941.65 7.361 33 878.17 2.198 1000
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1H NMR 89.56 MHz C12 H11 N O 0.045 g : 0.5 ml CDCl3 N-(2-naphthyl)acetamide Assign. Shift(ppm)
A 8.15 B 8.04 C 7.83 to 7.58 D 7.54 to 7.20 E 2.171
Hz ppm Int.730.75 8.160 69 730.19 8.154 70 729.25 8.143 74 729.13 8.142 74 697.69 7.791 44 695.31 7.764 88 692.94 7.738 55 691.69 7.724 62 689.50 7.699 65 687.06 7.672 170 671.94 7.503 74 669.88 7.480 91 668.00 7.459 32 665.88 7.436 118 665.06 7.426 112 663.31 7.407 103 661.13 7.382 105 660.19 7.372 79 658.19 7.350 62 655.88 7.324 92 194.50 2.172 1000
in CDCl3
KBr disc
nujol mull
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