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MassMS-NW-2361 N-benzoyl-DL-phenylalanine 2-naphthylamide C26H22N2O2 (Mass of molecular ion: 394)
Source Temperature: 250 °C Sample Temperature: 270 °C Direct, 75 eV
18.0 3.4 27.0 1.2 28.0 3.9 39.0 2.5 50.0 2.5 51.0 6.0 52.0 1.1 63.0 2.3 65.0 2.9 71.5 1.0 74.0 1.0 75.0 1.5 76.0 2.8 77.0 28.1 78.0 3.2 89.0 2.3 90.0 1.0 91.0 27.9 92.0 2.6 102.0 1.5 103.0 5.6 104.0 5.4 105.0 84.9 106.0 7.1 114.0 1.1 115.0 10.4 116.0 4.4 117.0 2.3 118.0 1.3 120.0 1.0 126.0 2.3 127.0 8.0 128.0 1.7 131.0 2.6 140.0 1.3 141.0 1.1 142.0 1.7 143.0 100.0 144.0 12.3 153.0 4.3 154.0 1.2 169.0 2.4 182.0 5.1 183.0 1.0 206.0 1.3 223.0 3.0 224.0 6.8 225.0 1.5 230.0 5.9 231.0 1.2 251.0 2.3 252.0 1.6 285.0 2.7 374.0 1.8
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C26 H22 N2 O2 0.043 g : 0.5 ml DMSO-d6 N-benzoyl-DL-phenylalanine 2-naphthylamide 
Assign. Shift(ppm)
A 10.5 B 8.87 C 8.354 D *1 7.90 E 7.88 F *1 7.86 G *1 7.84 J 7.684 K 7.54 L 7.48 M *2 7.47 N *2 7.42 P 7.313 Q 7.204 R 4.957 S 3.21
Hz ppm Int.4205.68 10.524 417 3551.96 8.888 237 3543.91 8.868 240 3339.67 8.357 342 3337.84 8.352 348 3161.82 7.912 325 3158.71 7.904 134 3156.51 7.899 416 3155.41 7.896 562 3153.58 7.891 481 3150.46 7.884 225 3148.45 7.879 637 3146.98 7.875 557 3137.83 7.852 502 3130.50 7.834 256 3129.95 7.832 254 3076.28 7.698 261 3074.27 7.693 257 3067.49 7.676 225 3065.47 7.671 222 3021.70 7.561 113 3016.94 7.549 97 3014.37 7.543 328 3011.99 7.537 132 3008.51 7.528 194 3007.04 7.525 311 3005.58 7.521 194 3000.27 7.508 203 2998.99 7.505 242 2994.77 7.494 822 2993.49 7.491 583 2992.39 7.488 437 2990.74 7.484 349 2988.36 7.478 773 2987.26 7.475 1000 2984.15 7.467 292 2981.77 7.461 145 2980.12 7.457 273 2978.84 7.454 180 2972.79 7.439 213 2971.51 7.436 185 2966.02 7.422 165 2964.73 7.419 253 2963.63 7.416 216 2957.96 7.402 130 2956.67 7.399 127 2930.11 7.332 292 2928.47 7.328 137 2922.79 7.314 563 2915.09 7.295 333 2887.62 7.226 124 2886.52 7.223 199 2885.24 7.220 132 2880.84 7.209 108 2879.01 7.204 273 2871.68 7.186 106 1983.88 4.965 97 1982.23 4.960 119 1978.93 4.952 98 1977.28 4.948 96 1291.51 3.232 196 1286.01 3.218 292 1275.57 3.192 171
KBr disc
nujol mull
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