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WebSite > CAS DataBase List >  5809-23-4More Spectrum > 2-(4-Diethylamino-2-hydroxybenzoyl)benzoic acid(5809-23-4)1HNMR

5809-23-4

2-(4-Diethylamino-2-hydroxybenzoyl)benzoic acid

Product Name 2-(4-Diethylamino-2-hydroxybenzoyl)benzoic acid

CAS5809-23-4

MFC18H19NO4

MW313.35

More

  • 5809-23-4_ms_1
    Mass

    MS-IW-3627          
    O-(4-diethylamino-2-hydroxybenzoyl)benzoic acid
    C18H19NO4           (Mass of molecular ion:    313)
    

       Source Temperature: 140 °C
       Sample Temperature: 110 °C
       Direct, 75 eV
    

          18.0       1.0
          29.0       1.9
          39.0       1.3
          53.0       1.1
          65.0       4.3
          77.0       2.2
          92.0       1.2
          93.0       2.9
         104.0       1.2
         105.0       1.8
         121.0       2.0
         122.0       2.3
         126.0       1.4
         133.5       2.6
         136.0       1.0
         139.0       3.3
         139.5       1.1
         140.0       1.8
         148.0       2.9
         149.0       8.8
         150.0       3.7
         156.5       2.0
         162.0       1.0
         164.0       1.0
         167.0       1.6
         168.0       1.4
         192.0       2.6
         195.0       2.1
         196.0       1.7
         210.0       1.0
         223.0       3.6
         224.0       3.2
         250.0       1.0
         252.0       5.5
         253.0       1.0
         268.0       3.8
         280.0      12.0
         281.0       2.4
         298.0     100.0
         299.0      19.4
         300.0       2.6
         312.0       2.5
         313.0      50.5
         314.0      10.4
         315.0       1.4
    

400 MHz in DMSO-d6

  • 5809-23-4_1hnmr_0

    1H NMR 399.65 MHz
    C18 H19 N O4 0.047 g : 0.5 ml DMSO-d6
    o-(4-diethylamino-2-hydroxybenzoyl)benzoic acid
    ChemicalStructure
        Assign.     Shift(ppm)
    A *1 12.61 B 7.983 C *2 7.685 D *2 7.617 E 7.386 F 6.811 G 6.183 J 6.089 K *1 3.6 L 3.379 M 1.097

         Hz     ppm     Int.
    

       5038.36  12.607    414
       3195.16   7.995    136
       3194.06   7.993    142
       3187.46   7.976    155
       3186.36   7.973    153
       3080.86   7.709     57
       3079.58   7.706     63
       3073.35   7.691    150
       3072.25   7.688    152
       3066.02   7.672    112
       3064.74   7.669    107
       3051.55   7.636    101
       3050.45   7.633    112
       3044.04   7.617    144
       3042.76   7.614    152
       3036.53   7.598     63
       3035.25   7.595     61
       2955.94   7.397    154
       2954.84   7.394    159
       2948.43   7.378    141
       2947.33   7.375    135
       2726.80   6.823    236
       2717.82   6.801    263
       2477.14   6.199    112
       2474.76   6.193    122
       2467.99   6.176    105
       2465.42   6.169    118
       2434.83   6.093    240
       2432.45   6.087    215
       1368.62   3.425     31
       1368.25   3.424     31
       1361.11   3.406    140
       1354.15   3.389    381
       1347.19   3.371    383
       1340.05   3.354    139
        452.79   1.133     30
        445.46   1.115    476
        438.50   1.098   1000
        431.54   1.080    446
    

in DMSO-d6

  • 5809-23-4_13cnmr_0

KBr disc

  • 5809-23-4_ir1_2

nujol mull

  • 5809-23-4_ir2_1