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4-(4-Bromophenyl)-4-piperidinol

Product Name 4-(4-Bromophenyl)-4-piperidinol

CAS57988-58-6

MFC11H14BrNO

MW256.14

¹³CNMR

Mass

MS-IW-7697          
4-(p-bromophenyl)-4-piperidinol
C11H14BrNO          (Mass of molecular ion:    255)

   Source Temperature: 180 °C
   Sample Temperature: 160 °C
   Direct, 75 eV

      15.0       1.7
      17.0       1.4
      18.0       7.3
      27.0       4.1
      28.0      13.4
      29.0       8.1
      30.0      34.2
      39.0       4.2
      41.0       5.4
      42.0     100.0
      43.0      21.4
      44.0      34.7
      45.0       1.5
      50.0       7.0
      51.0       9.4
      52.0       1.9
      53.0       2.6
      54.0       1.4
      55.0       3.5
      56.0      46.3
      57.0      55.1
      58.0       5.3
      60.0       2.9
      62.0       1.9
      63.0       7.0
      63.5       1.5
      64.0       3.3
      65.0       3.4
      68.0       5.6
      70.0       1.9
      71.0       1.2
      72.0       1.4
      74.0       4.6
      75.0      10.2
      76.0       8.5
      76.5       1.0
      77.0      12.1
      77.5       2.8
      78.0       3.1
      78.5       1.8
      79.0       2.0
      80.0       5.7
      81.0       4.2
      82.0      23.7
      83.0       1.9
      84.0       3.9
      86.0       1.2
      87.0       1.2
      87.5       1.5
      88.0       1.3
      89.0       4.4
      90.0       4.4
      91.0       6.1
      98.0       2.6
      99.0       4.3
     100.0       1.2
     101.0       5.9
     102.0      11.4
     103.0       4.7
     104.0       3.1
     105.0       1.6
     114.0       2.5
     115.0      16.3
     116.0       9.8
     117.0       3.8
     117.5       1.0
     118.0       1.3
     126.0       4.0
     127.0      15.1
     128.0      16.8
     129.0      37.0
     130.0      13.4
     131.0       7.1
     132.0       2.4
     133.0       2.0
     141.0       1.0
     143.0       2.6
     153.0       2.2
     154.0       9.3
     155.0       6.5
     156.0       4.3
     157.0       6.1
     158.0      36.9
     159.0       8.2
     169.0       6.8
     171.0       6.4
     180.0       1.1
     181.0       2.6
     182.0       4.4
     183.0      14.2
     184.0       5.4
     185.0      11.7
     186.0       2.0
     193.0       2.1
     195.0       3.7
     196.0       3.1
     197.0       2.0
     198.0       8.5
     199.0       2.0
     200.0       5.6
     201.0       1.2
     208.0      11.0
     209.0       5.0
     210.0      15.3
     211.0       6.1
     212.0       5.4
     213.0       1.6
     222.0       2.0
     223.0       1.0
     224.0       2.2
     225.0       2.8
     226.0       1.9
     227.0       8.1
     228.0       2.1
     229.0       5.9
     233.0      31.6
     234.0       5.7
     235.0      31.8
     236.0      40.0
     237.0      81.4
     238.0      45.3
     239.0      81.1
     240.0      11.9
     241.0       1.5
     250.0       1.3
     251.0       1.0
     252.0       1.7
     253.0       1.0
     254.0       5.0
     255.0      27.3
     256.0       8.4
     257.0      27.3
     258.0       3.6
     267.0       2.4
     269.0       2.4

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₁ H₁₄ Br N O	0.039 g : 0.5 ml DMSO-d₆
4-(p-bromophenyl)-4-piperidinol

    Assign.     Shift(ppm)

      A             7.496
      B             7.423
      C             4.96
      D             2.907
      E             2.716
      F             1.82
      G             1.752
      J             1.487

     Hz     ppm     Int.

   3003.54   7.516     96
   3001.22   7.510    558
   2999.39   7.506    241
   2994.51   7.493    312
   2992.55   7.488   1000
   2990.23   7.483    205
   2972.53   7.438    185
   2970.34   7.433    937
   2968.38   7.428    309
   2963.50   7.416    230
   2961.67   7.411    556
   2959.23   7.405    103
   1982.54   4.961    106
   1176.27   2.944    129
   1174.19   2.939    155
   1170.41   2.929     54
   1169.56   2.927     53
   1164.31   2.914    316
   1162.23   2.909    329
   1152.22   2.884    211
   1150.15   2.878    193
   1090.09   2.728    265
   1079.35   2.701    209
   1078.13   2.698    204
   1077.76   2.697    204
    715.21   1.790    154
    710.69   1.779    168
    702.27   1.758    276
    698.12   1.747    273
    690.06   1.727    179
    685.42   1.716    158

in DMSO-d6

KBr disc

nujol mull

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