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MassMS-NW-6105 1-p-menthen-4-ol C10H18O (Mass of molecular ion: 154)
Source Temperature: 260 °C Sample Temperature: 190 °C Reservoir, 75 eV
15.0 1.0 18.0 1.3 27.0 11.6 28.0 1.7 29.0 5.4 31.0 1.9 39.0 10.3 40.0 2.8 41.0 23.2 42.0 2.7 43.0 29.1 44.0 1.3 45.0 2.0 51.0 2.6 52.0 1.4 53.0 9.2 54.0 1.5 55.0 17.3 56.0 1.3 57.0 2.4 58.0 2.8 59.0 3.6 65.0 3.1 66.0 1.3 67.0 13.8 68.0 15.3 69.0 21.3 70.0 3.8 71.0 100.0 72.0 5.2 77.0 8.9 78.0 1.6 79.0 4.8 80.0 1.1 81.0 12.5 82.0 3.4 83.0 10.2 84.0 1.8 85.0 2.0 86.0 27.3 87.0 2.3 91.0 7.7 92.0 6.9 93.0 43.5 94.0 4.6 95.0 6.0 96.0 1.5 97.0 1.7 98.0 1.8 105.0 1.4 107.0 1.7 109.0 1.5 110.0 4.4 111.0 49.9 112.0 4.0 119.0 2.2 121.0 4.8 125.0 2.5 136.0 8.8 137.0 1.5 139.0 2.9 154.0 14.9 155.0 1.8
400 MHz in CDCl3
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1H NMR 399.65 MHz C10 H18 O 0.05 ml : 0.5 ml CDCl3 1-p-menthen-4-ol 
Assign. Shift(ppm)
A 5.291 B *1 2.15 C *1 1.91 D 1.68 E 1.64 F 1.55 G *2 0.944 J *2 0.916 assigned by C-H COSY
Hz ppm Int.2120.00 5.305 42 2116.46 5.296 107 2115.23 5.293 116 2113.89 5.290 114 2113.04 5.288 115 2111.69 5.284 108 853.64 2.136 119 770.51 1.928 87 768.43 1.923 82 767.46 1.921 80 766.97 1.920 79 763.67 1.911 90 761.96 1.907 91 760.50 1.903 81 671.51 1.681 631 667.72 1.671 315 660.64 1.654 223 653.56 1.636 143 634.28 1.588 74 628.30 1.573 103 623.41 1.560 95 621.70 1.556 55 621.09 1.555 55 617.31 1.545 68 616.70 1.544 67 615.11 1.540 57 610.23 1.527 46 604.37 1.513 39 380.62 0.953 915 373.78 0.936 904 369.75 0.926 1000 362.79 0.908 973
in CDCl3
liquid film
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