L-Lysine

Mass

MS-IW-7274          
L-lysine
C6H14N2O2           (Mass of molecular ion:    146)

   Source Temperature: 210 °C
   Sample Temperature: 190 °C
   Direct, 75 eV

      15.0       2.6
      16.0       6.3
      17.0      17.5
      18.0      70.6
      26.0       7.8
      27.0      24.4
      28.0      52.0
      29.0      11.7
      30.0      95.4
      31.0       2.7
      37.0       1.2
      38.0       2.4
      39.0      13.0
      40.0       6.2
      41.0      29.4
      42.0      20.0
      43.0      42.8
      44.0      38.2
      45.0       4.4
      46.0       1.4
      50.0       3.8
      51.0       5.9
      52.0      14.3
      53.0       8.9
      54.0      18.3
      55.0      33.6
      56.0     100.0
      57.0      20.4
      58.0       6.1
      59.0       6.0
      65.0       3.4
      66.0       5.7
      67.0      11.4
      68.0       7.1
      69.0       6.5
      70.0      19.4
      71.0      15.3
      72.0      66.6
      73.0       6.6
      74.0      13.1
      75.0       3.7
      77.0       2.1
      78.0       3.7
      79.0      13.8
      80.0       8.1
      81.0       7.8
      82.0      35.7
      83.0      83.6
      84.0      74.6
      85.0       6.7
      86.0       1.5
      87.0       1.9
      88.0       1.9
      89.0       1.8
      92.0       2.0
      93.0       6.9
      94.0       1.6
      95.0       1.7
      96.0       1.1
      97.0       1.8
      98.0       3.0
      99.0      16.4
     100.0       9.3
     101.0       3.8
     104.0       3.2
     107.0       1.7
     108.0       2.8
     109.0       2.4
     110.0      11.4
     111.0      18.9
     112.0       3.4
     117.0       2.5
     126.0       1.5
     127.0       2.8
     128.0       8.8
     129.0      10.8
     130.0       4.7
     147.0       1.7

Assign. Shift(ppm) B 3.756 C 3.029 D 1.95 to 1.43 THE SOLVENT SIGNAL REMOVED.

     Hz     ppm     Int.

    342.94   3.830    384
    337.25   3.766    907
    331.19   3.698    554
    279.25   3.119    559
    272.56   3.044   1000
    265.00   2.959    901
    167.38   1.869    691
    164.69   1.839    535
    163.94   1.831    542
    161.63   1.805    666
    157.81   1.763    544
    157.44   1.758    547
    157.13   1.755    545
    155.13   1.733    522
    149.19   1.666    547
    148.75   1.661    546
    148.19   1.655    539
    144.38   1.613    628
    143.00   1.597    547
    142.50   1.592    540
    141.75   1.583    540