400 MHz in D2O
90 MHz in D2O
-
1H NMR 399.65 MHz C6 H14 N2 O2 0.037 g : 0.5 ml D2O L-lysine dihydrochloride 
Assign. Shift(ppm)
B 4.117 C 3.034 D *1 2.03 E *1 1.97 F 1.741 G 1.54 THE SOLVENT SIGNAL REMOVED.
Hz ppm Int.1651.73 4.133 449 1645.39 4.118 867 1642.46 4.110 157 1639.04 4.102 453 1220.34 3.054 626 1212.77 3.035 1000 1204.96 3.016 640 829.96 2.077 145 829.71 2.077 145 824.46 2.063 147 824.10 2.063 143 820.92 2.055 231 818.85 2.049 211 815.19 2.040 376 812.74 2.034 189 810.30 2.028 344 804.44 2.013 567 798.22 1.998 499 793.33 1.986 274 791.38 1.981 286 787.60 1.971 344 783.08 1.960 197 782.71 1.959 197 781.13 1.955 258 773.32 1.935 145 712.28 1.783 223 704.47 1.763 710 696.78 1.744 982 689.09 1.725 795 681.52 1.706 320 636.47 1.593 213 630.62 1.578 229 629.03 1.574 282 625.85 1.566 250 623.29 1.560 298 620.97 1.554 338 618.41 1.548 300 615.48 1.541 304 613.04 1.534 372 610.47 1.528 268 607.79 1.521 292 605.10 1.515 310 602.54 1.508 252 601.07 1.504 211 600.10 1.502 233 597.17 1.495 235 594.60 1.488 189 589.36 1.475 161
-
1H NMR 89.56 MHz C6 H14 N2 O2 0.042 g : 0.5 ml D2O L-lysine dihydrochloride Assign. Shift(ppm)
B 4.075 C 3.024 D 1.99 E 1.79 to 1.45 THE SOLVENT SIGNAL REMOVED.
Hz ppm Int.371.50 4.149 435 371.38 4.147 435 365.50 4.082 1000 359.25 4.012 581 278.69 3.112 443 278.38 3.109 443 278.00 3.105 423 271.94 3.037 842 264.88 2.958 607 264.50 2.954 623 182.75 2.041 518 181.00 2.021 516 180.25 2.013 494 177.63 1.984 476 177.00 1.977 486 174.63 1.950 844 172.94 1.931 468 168.38 1.881 494 168.19 1.878 494 157.69 1.761 630 157.19 1.756 626 156.38 1.747 593 156.00 1.742 593 155.44 1.736 609 154.94 1.731 609 154.56 1.726 626 151.75 1.695 709 148.00 1.653 889 147.69 1.650 883 146.25 1.633 913 146.06 1.631 913 144.69 1.616 765 142.25 1.589 713 140.56 1.570 617 140.25 1.566 615
in D2O
KBr disc
nujol mull
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