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MS2015-05290CW 2'-nitroacetanilide C8H8N2O3 (Mass of molecular ion: 180)
Source Temperature: 250 °C Sample Temperature: 20 °C Direct, 70 eV
17.0 1.5 18.0 6.2 28.0 2.6 38.0 1.3 39.0 2.9 43.0 24.4 50.0 1.5 51.0 2.3 52.0 3.7 62.0 1.2 63.0 5.3 64.0 4.4 65.0 13.8 66.0 1.5 76.0 1.1 77.0 1.9 78.0 1.5 80.0 7.0 90.0 3.4 91.0 3.2 92.0 27.6 93.0 2.5 108.0 12.5 121.0 4.3 122.0 2.4 132.0 1.0 134.0 7.9 138.0 100.0 139.0 7.5 180.0 20.5 181.0 2.0
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H8 N2 O3 0.046 g : 0.5 ml CDCl3 2'-nitroacetanilide Assign. Shift(ppm)
A 10.3 B 8.76 C 8.20 D 7.65 F 2.296
Hz ppm Int.
790.21 8.824 59 788.89 8.809 57 781.71 8.729 68 780.25 8.713 65 740.26 8.266 53 738.72 8.249 57 731.84 8.172 66 730.22 8.154 69 686.79 7.669 42 686.43 7.665 41 685.11 7.650 54 649.73 7.255 57 643.87 7.190 45 642.55 7.175 69 641.31 7.161 46 635.38 7.095 36 205.74 2.298 1000
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