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MS-NW-1652 4'-nitroacetanilide C8H8N2O3 (Mass of molecular ion: 180)
Source Temperature: 190 °C Sample Temperature: 180 °C Direct, 75 eV
15.0 5.9 18.0 2.8 28.0 2.1 30.0 6.4 37.0 1.2 38.0 4.3 39.0 7.1 40.0 1.0 41.0 2.4 42.0 2.0 43.0 97.3 44.0 2.2 50.0 3.4 51.0 2.4 52.0 4.0 53.0 2.1 61.0 1.1 62.0 2.6 63.0 8.9 64.0 7.8 65.0 22.8 66.0 2.7 74.0 1.1 75.0 1.5 76.0 1.9 79.0 1.0 80.0 4.9 90.0 1.9 91.0 3.3 92.0 26.4 93.0 2.3 105.0 1.1 108.0 26.5 109.0 2.0 122.0 5.6 138.0 100.0 139.0 7.5 180.0 33.4 181.0 3.3
400 MHz in DMSO-d6
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1H NMR 399.65 MHz C8 H8 N2 O3 0.036 g : 0.5 ml DMSO-d6 4'-nitroacetanilide Assign. Shift(ppm)
A 10.57 B 8.211 C 7.834 D 2.143
Hz ppm Int.
4223.48 10.568 99 3289.49 8.231 35 3286.44 8.224 266 3284.45 8.219 91 3279.27 8.206 97 3277.28 8.201 293 3274.23 8.193 37 3138.12 7.853 41 3135.22 7.845 293 3133.24 7.840 95 3130.49 7.834 22 3128.05 7.827 90 3126.07 7.823 253 3123.02 7.815 32 856.48 2.144 1000
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