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Diethoxy(methyl)vinylsilane

Product Name Diethoxy(methyl)vinylsilane

CAS5507-44-8

MFC7H16O2Si

MW160.29


  • Mass 

    MS-IW-6964          
diethoxymethylvinylsilane
C7H16O2Si           (Mass of molecular ion:    160)


       Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV


          26.0       1.5
      27.0       2.6
      28.0       2.3
      29.0       1.5
      43.0       2.3
      45.0      11.0
      47.0       1.1
      55.0       1.1
      59.0       1.6
      60.0       1.0
      61.0      14.8
      62.0       1.7
      63.0       7.7
      65.0       1.0
      71.0       6.7
      72.0       1.5
      73.0       7.6
      77.0      15.8
      78.0       1.0
      85.0       1.1
      87.0       5.7
      88.0       1.5
      89.0      22.1
      90.0       1.9
      91.0       4.6
      99.0       1.7
     101.0      29.0
     102.0       2.9
     103.0       2.3
     105.0       9.6
     115.0      20.3
     116.0       2.5
     117.0      10.0
     118.0       1.3
     133.0      16.4
     134.0       1.7
     145.0     100.0
     146.0      11.8
     147.0       4.4

parameter in CDCl3

400 MHz in CDCl3


  • 1H NMR 300 MHz
    C7 H16 O2 Si 0.05 ml : 0.5 ml CDCl3
    diethoxymethylvinylsilane
    ChemicalStructure 
        Parameter     ppm  Hz
    
      D(A)         6.077
      D(B)         6.030
      D(C)         5.911
       J(A,B)         14.8
       J(A,C)          5.6
       J(B,C)         19.1
     
      D(D)         3.786
      D(E)         1.225
       J(D,E)          7.2
     
      D(F)         0.196
  

         Hz     ppm     Int.


       1830.50   6.102     32
   1823.57   6.079    190
   1815.92   6.053    159
   1806.46   6.022    191
   1791.78   5.973     55
   1789.91   5.966     17
   1783.09   5.944    139
   1775.61   5.919     91
   1765.88   5.886     50
   1758.29   5.861     39
   1146.66   3.822    160
   1139.46   3.798    490
   1132.31   3.774    500
   1125.11   3.750    170
    374.68   1.249    507
    367.53   1.225    982
    360.32   1.201    489
     58.80   0.196   1000


  • 1H NMR 399.65 MHz
    C7 H16 O2 Si 0.05 ml : 0.5 ml CDCl3
    diethoxymethylvinylsilane
    ChemicalStructure 
        Assign.     Shift(ppm)
    
      A             6.08
      B             6.06
      C             5.911
      D             3.786
      E             1.225
      F             0.196
  

         Hz     ppm     Int.


       2443.73   6.115     33
   2438.11   6.101     63
   2428.96   6.078    178
   2426.03   6.071    143
   2423.46   6.064    186
   2407.96   6.026     38
   2406.86   6.023    205
   2392.09   5.986     92
   2371.09   5.933    166
   2365.48   5.919    140
   2352.05   5.886     76
   2346.44   5.872     71
   1524.29   3.815    202
   1518.68   3.801     51
   1517.21   3.797    543
   1511.72   3.783     52
   1510.13   3.779    586
   1503.17   3.762    253
    496.83   1.244    572
    489.75   1.226   1000
    482.79   1.209    621
     82.40   0.207     60
     78.61   0.197    942
     75.20   0.189     64

in CDCl3



liquid film





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