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MS-NW-9655 trimethoxy(vinyl)silane C5H12O3Si (Mass of molecular ion: 148)
Source Temperature: 260 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.0 28.0 2.2 45.0 3.6 47.0 1.5 59.0 11.7 60.0 3.4 61.0 10.5 73.0 1.0 77.0 2.6 85.0 2.2 86.0 2.4 87.0 14.6 88.0 1.4 90.0 10.4 91.0 65.2 92.0 5.3 93.0 3.1 105.0 7.7 106.0 1.0 107.0 22.6 108.0 1.7 115.0 1.7 116.0 1.7 117.0 20.7 118.0 30.3 119.0 5.4 120.0 14.9 121.0 100.0 122.0 9.2 123.0 4.3 130.0 1.4 133.0 19.7 134.0 1.9 147.0 3.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C5 H12 O3 Si 0.05 ml : 0.5 ml CDCl3 trimethoxy(vinyl)silane Assign. Shift(ppm)
A 6.173 B 6.052 C 5.876 D 3.579 J(A,C)=14.8HZ J(A,B)=4.0HZ J(B,C)=20.8HZ
Hz ppm Int.
2477.17 6.199 116 2473.02 6.188 129 2462.52 6.162 135 2458.37 6.152 152 2423.22 6.064 96 2419.07 6.053 99 2402.47 6.012 182 2398.32 6.002 156 2362.18 5.911 186 2347.53 5.874 145 2341.43 5.859 100 2326.78 5.823 87 1500.98 3.756 29 1430.54 3.580 1000 1428.47 3.575 345 1357.79 3.398 30
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