2-Chloro-3-nitropyridine

Mass

MS-NW-7243          
2-chloro-3-nitropyridine
C5H3ClN2O2          (Mass of molecular ion:    158)

   Source Temperature: 200 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      26.0       3.8
      27.0       1.0
      28.0       3.0
      30.0       7.5
      36.0       1.1
      37.0       3.1
      38.0       4.8
      39.0       4.6
      46.0       1.2
      47.0       1.3
      49.0       4.0
      50.0      20.2
      51.0      18.3
      52.0       3.8
      61.0       3.4
      62.0       5.7
      63.0       1.8
      64.0       2.3
      75.0       4.1
      76.0      57.9
      77.0       5.2
      84.0       3.5
      85.0      20.6
      86.0       3.4
      87.0       6.9
     100.0       9.1
     102.0       3.0
     112.0     100.0
     113.0       6.2
     114.0      32.7
     115.0       2.0
     158.0      48.7
     159.0       3.6
     160.0      16.0
     161.0       1.2

Assign. Shift(ppm) A 8.644 B 8.251 C 7.507 J(A,B)=1.8HZ J(A,C)=4.7HZ J(B,C)=8.0HZ

     Hz     ppm     Int.

    777.56   8.683    455
    775.81   8.663    508
    772.88   8.630    509
    771.13   8.611    536
    744.31   8.311    570
    742.56   8.292    533
    736.31   8.222    714
    734.50   8.202    651
    678.25   7.574   1000
    676.38   7.553     64
    675.75   7.546     64
    673.56   7.521    949
    670.25   7.484    828
    668.38   7.463     60
    667.19   7.450     64
    665.50   7.431    754