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Dimethyl 2,6-Pyridinedicarboxylate

Product Name Dimethyl 2,6-Pyridinedicarboxylate

CAS5453-67-8

MFC9H9NO4

MW195.17

¹³CNMR

Mass

MS-IW-2954          
dimethyl 2,6-pyridinedicarboxylate
C9H9NO4             (Mass of molecular ion:    195)

   Source Temperature: 200 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      15.0       8.6
      26.0       1.1
      28.0       1.5
      29.0       1.1
      39.0       3.4
      42.0       1.3
      50.0       5.6
      51.0       4.2
      52.0       1.1
      52.5       1.5
      53.0       1.8
      59.0      13.8
      65.0       6.3
      66.0       1.4
      75.0       1.4
      76.0       3.9
      77.0      13.9
      78.0       5.1
      83.0       1.1
      92.0       7.7
      93.0       3.3
     104.0       1.3
     105.0      49.5
     106.0       5.9
     136.0      27.3
     137.0     100.0
     138.0       8.1
     164.0       7.9
     165.0      15.6
     166.0       1.5
     195.0       2.0

parameter in CDCl3

in CDCl3

¹H NMR	300 MHz
C₉ H₉ N O₄	5 mol% in CDCl₃
dimethyl 2,6-pyridinedicarboxylate

    Parameter     ppm  Hz

      D(A)         8.31
      D(B)         8.04
       J(A,B)          8.10
     
      D(C)         4.03
     
     DEADY,L.W. ET AL. ORG.MAGN.RESON. 7, 41 (1975)

     Hz     ppm     Int.

   2497.12   8.324    108
   2489.19   8.297    150
   2419.68   8.066     51
   2411.99   8.040     49
   2411.23   8.037     48
   2403.54   8.012     34
   1209.02   4.030   1000

in CDCl3

KBr disc

nujol mull

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