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MS-NW-6384 diisopentylamine C10H23N (Mass of molecular ion: 157)
Source Temperature: 270 °C Sample Temperature: 190 °C Reservoir, 75 eV
18.0 1.5 27.0 6.5 28.0 3.7 29.0 10.9 30.0 45.8 39.0 4.0 41.0 12.9 42.0 5.4 43.0 34.5 44.0 61.8 45.0 1.9 55.0 3.9 56.0 3.4 57.0 2.0 58.0 2.3 69.0 2.0 70.0 3.9 71.0 8.0 72.0 1.5 84.0 1.1 86.0 1.7 98.0 3.0 100.0 100.0 101.0 6.8 128.0 1.5 157.0 3.5
90 MHz in CDCl3
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1H NMR 89.56 MHz C10 H23 N 0.04 ml : 0.5 ml CDCl3 diisopentylamine Assign. Shift(ppm)
A 2.606 B 1.56 C 1.38 D 1.14 E 0.901
Hz ppm Int.
241.06 2.692 127 233.75 2.610 137 231.81 2.589 53 226.38 2.528 157 152.69 1.705 23 145.81 1.629 33 139.75 1.561 35 133.13 1.487 90 127.63 1.426 80 125.94 1.407 121 123.75 1.382 43 121.44 1.356 42 120.31 1.344 39 118.75 1.326 134 112.88 1.261 38 111.44 1.245 31 102.00 1.139 87 83.38 0.931 1000 77.31 0.864 764
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