3-Methyl-4-nitroanisole

Mass

MS-NW-6903          
3-methyl-4-nitroanisole
C8H9NO3             (Mass of molecular ion:    167)

   Source Temperature: 120 °C
   Sample Temperature:  70 °C
   Direct, 75 eV

      15.0       4.6
      18.0       2.3
      26.0       1.6
      27.0       4.7
      28.0       3.7
      29.0       1.9
      30.0       3.7
      37.0       1.7
      38.0       5.3
      39.0      16.8
      40.0       2.7
      41.0       6.7
      42.0       1.3
      43.0       2.0
      45.0       1.3
      50.0       9.1
      51.0      21.7
      52.0      17.4
      53.0       8.8
      54.0       1.5
      55.0       3.9
      59.0       1.9
      61.0       1.6
      62.0       5.1
      63.0      13.8
      64.0       4.6
      65.0      21.2
      66.0       6.5
      67.0       3.6
      68.0       1.4
      74.0       2.6
      75.0       2.3
      76.0       2.6
      77.0      29.9
      78.0      29.8
      79.0       7.6
      80.0       3.8
      81.0       2.0
      86.0       1.0
      89.0       8.1
      90.0       8.3
      91.0      28.1
      92.0      10.1
      93.0       2.2
      94.0       6.8
      95.0      26.6
      96.0       2.3
     105.0       4.5
     106.0      14.1
     107.0       6.4
     108.0       5.8
     109.0       5.0
     120.0       2.3
     121.0       8.4
     122.0      20.7
     123.0       2.9
     134.0       1.2
     135.0       3.3
     136.0       5.3
     137.0       8.2
     138.0       1.5
     150.0     100.0
     151.0       9.9
     152.0       1.3
     167.0      84.9
     168.0       8.4
     169.0       1.0

Assign. Shift(ppm) A 8.076 B 6.797 C 6.78 D 3.879 E 2.627

     Hz     ppm     Int.

   3232.18   8.088    133
   3223.27   8.066    138
   2723.39   6.815     56
   2720.58   6.808     80
   2714.23   6.792     40
   2711.67   6.786    105
   2709.11   6.779    140
   2706.91   6.774     66
   2706.30   6.772     72
   1550.42   3.880   1000
   1049.80   2.627    611