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MassMS-NW-3738 m-anisidine C7H9NO (Mass of molecular ion: 123)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 2.4 17.0 1.0 18.0 4.7 27.0 3.8 28.0 5.9 37.0 1.4 38.0 4.0 39.0 10.2 40.0 2.5 41.0 5.4 42.0 1.4 50.0 2.3 51.0 4.0 52.0 8.9 53.0 14.5 54.0 4.0 61.0 1.1 61.5 1.7 62.0 2.0 63.0 4.4 64.0 2.8 65.0 10.1 66.0 14.2 67.0 2.8 68.0 1.5 77.0 4.0 78.0 2.6 79.0 3.7 80.0 31.4 81.0 2.3 91.0 1.2 92.0 7.0 93.0 42.6 94.0 45.8 95.0 7.9 104.0 1.0 105.0 1.3 106.0 1.6 107.0 2.1 122.0 7.0 123.0 100.0 124.0 8.3
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H9 N O 0.04 ml : 0.5 ml CDCl3 m-anisidine 
Assign. Shift(ppm)
A 7.03 B *1 6.30 C *1 6.24 D 6.21 E 3.718 F 3.59
Hz ppm Int.638.19 7.126 44 631.50 7.052 31 630.13 7.036 73 629.19 7.026 53 622.75 6.954 55 621.75 6.943 65 570.00 6.365 35 569.06 6.354 53 567.75 6.340 47 566.75 6.329 76 564.94 6.308 54 563.94 6.297 44 562.75 6.284 102 561.75 6.273 66 560.31 6.257 60 558.63 6.238 75 557.75 6.228 77 556.06 6.209 249 554.44 6.191 130 553.31 6.179 34 333.00 3.719 1000 321.25 3.587 233
in CDCl3
CCl4 solution
liquid film
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