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MS-NW-1537 p-anisidine C7H9NO (Mass of molecular ion: 123)
Source Temperature: 240 °C Sample Temperature: 180 °C Reservoir, 75 eV
15.0 1.8 26.0 1.5 27.0 3.7 28.0 5.6 37.0 1.0 38.0 2.2 39.0 6.8 40.0 1.2 41.0 3.5 50.0 1.8 51.0 3.3 52.0 10.5 53.0 14.4 54.0 3.8 61.0 2.6 62.0 1.7 63.0 3.2 64.0 1.7 65.0 6.7 66.0 1.3 78.0 1.2 79.0 2.0 80.0 36.9 81.0 2.5 92.0 2.0 95.0 2.3 108.0 100.0 109.0 7.2 122.0 2.8 123.0 80.5 124.0 6.9
90 MHz in CDCl3
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1H NMR 89.56 MHz C7 H9 N O 0.048 g : 0.5 ml CDCl3 p-anisidine Assign. Shift(ppm)
A 6.71 B 6.63 C 3.720 D 3.40
Hz ppm Int.
609.19 6.803 32 608.75 6.798 35 608.13 6.791 35 605.81 6.765 30 602.69 6.730 40 599.75 6.697 264 597.50 6.672 109 595.38 6.648 293 592.50 6.616 47 589.31 6.581 35 587.06 6.555 38 586.38 6.548 40 585.94 6.543 38 333.13 3.720 1000 304.31 3.398 454
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