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MS-IW-0553 6-chloro-3-pyridinamine C5H5ClN2 (Mass of molecular ion: 128)
Source Temperature: 250 °C Sample Temperature: 160 °C Reservoir, 75 eV
18.0 2.0 28.0 3.5 36.0 1.0 37.0 2.9 38.0 4.7 39.0 9.6 40.0 3.8 41.0 8.1 42.0 2.0 49.0 1.1 50.0 1.3 51.0 1.3 52.0 3.0 63.0 1.0 64.0 3.6 65.0 3.5 66.0 31.0 67.0 4.0 72.0 1.0 73.0 5.5 74.0 1.7 75.0 2.7 76.0 1.2 92.0 1.9 93.0 40.2 94.0 2.6 100.0 2.8 101.0 7.6 102.0 1.4 103.0 2.5 127.0 1.3 128.0 100.0 129.0 7.7 130.0 32.4 131.0 2.3
400 MHz in CDCl3
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1H NMR 399.65 MHz C5 H5 Cl N2 0.028 g : 0.5 ml CDCl3 6-chloro-3-pyridinamine Assign. Shift(ppm)
A 7.838 B 7.074 C 6.967 D 3.84
Hz ppm Int.
3134.16 7.843 755 3131.23 7.835 765 2832.28 7.087 698 2823.73 7.066 1000 2789.55 6.980 626 2786.50 6.973 621 2781.01 6.959 441 2778.08 6.952 430 1533.20 3.837 264
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