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535-15-9

ETHYL DICHLOROACETATE

Product Name ETHYL DICHLOROACETATE

CAS535-15-9

MFC4H6Cl2O2

MW157

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  • 535-15-9_ms_1
    Mass 

    MS-NW-6376          
ethyl dichloroacetate
C4H6Cl2O2           (Mass of molecular ion:    156)


       Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV


          15.0       1.3
      26.0       1.6
      27.0      16.3
      28.0       7.8
      29.0     100.0
      30.0       2.5
      36.0       1.7
      41.0       2.5
      43.0       1.3
      45.0       1.5
      47.0       1.2
      48.0       3.6
      50.0       1.2
      76.0       3.3
      77.0       4.2
      78.0       1.1
      79.0       1.4
      83.0       9.5
      85.0       6.0
      87.0       1.0
     111.0       2.3
     113.0       1.9

parameter in CDCl3

parameter neat

  • 535-15-9_1hnmr_2

    1H NMR 300 MHz
    C4 H6 Cl2 O2 0.05 ml : 0.5 ml CDCl3
    ethyl dichloroacetate
    ChemicalStructure 
        Parameter     ppm  Hz
    
      D(A)         5.963
     
      D(B)         4.337
      D(C)         1.359
       J(B,C)          7.1
  

         Hz     ppm     Int.


       1788.90   5.963    665
   1311.80   4.373    162
   1304.74   4.349    490
   1297.64   4.325    498
   1290.54   4.302    170
    414.80   1.383    503
    407.70   1.359   1000
    400.59   1.335    488

  • 535-15-9_1hnmr_0

    1H NMR 300 MHz
    C4 H6 Cl2 O2 neat
    ethyl dichloroacetate
    ChemicalStructure 
        Parameter     ppm  Hz
    
      D(A)         1.334
      D(B)         4.316
       J(A,B)          7.12
     
      D(C)         6.065
     
     RATTET,L.S. & GOLDSTEIN,J.H. J.PHYS.CHEM. 73, 4400(1969)
  

         Hz     ppm     Int.


       1819.50   6.065    674
   1305.51   4.352    164
   1298.42   4.328    501
   1291.30   4.304    507
   1284.21   4.281    172
    407.30   1.358    513
    400.21   1.334   1000
    393.08   1.310    494

in CDCl3

  • 535-15-9_13cnmr_0

liquid film

  • 535-15-9_ir1_0

4880 A,200 M,liquid

  • 535-15-9_raman_0

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