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MS-IW-6144 ethyl trichloroacetate C4H5Cl3O2 (Mass of molecular ion: 190)
Source Temperature: 200 °C Sample Temperature: 150 °C Reservoir, 75 eV
15.0 1.4 26.0 1.8 27.0 21.8 28.0 4.6 29.0 100.0 30.0 5.1 36.0 1.8 43.0 2.8 44.0 2.9 45.0 2.9 47.0 5.7 49.0 2.3 63.0 3.6 65.0 1.2 73.0 1.6 82.0 9.1 83.0 8.7 84.0 5.8 85.0 5.6 86.0 1.0 99.0 1.3 110.0 3.7 111.0 6.3 112.0 2.5 113.0 4.1 117.0 31.1 119.0 30.0 121.0 9.7 123.0 1.0 127.0 1.1 145.0 1.6 147.0 2.3 149.0 1.3 155.0 6.7 157.0 4.3
parameter neat
400 MHz in CDCl3
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1H NMR 300 MHz C4 H5 Cl3 O2 neat ethyl trichloroacetate Parameter ppm Hz
D(A) 1.399 D(B) 4.415 J(A,B) 7.11 RATTET,L.S. & GOLDSTEIN,J.H. J.PHYS.CHEM. 73, 4400 (1969)
Hz ppm Int.
1335.22 4.451 163 1328.12 4.427 494 1320.99 4.403 502 1313.89 4.380 171 426.77 1.423 507 419.70 1.399 1000 412.60 1.375 491
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1H NMR 399.65 MHz C4 H5 Cl3 O2 0.05 ml : 0.5 ml CDCl3 ethyl trichloroacetate Assign. Shift(ppm)
A 4.439 B 1.419
Hz ppm Int.
1785.03 4.467 216 1777.95 4.449 573 1770.75 4.431 590 1763.67 4.414 228 574.46 1.438 598 571.90 1.432 21 567.26 1.420 1000 560.18 1.402 597
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