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Ethyl 2-chloropropionate

Product Name Ethyl 2-chloropropionate

CAS535-13-7

MFC5H9ClO2

MW136.58

Mass

MS-NW-1361          
ethyl 2-chloropropionate
C5H9ClO2            (Mass of molecular ion:    136)

   Source Temperature: 260 °C
   Sample Temperature: 180 °C
   Reservoir, 75 eV

      15.0       2.2
      26.0       5.2
      27.0      40.4
      28.0      17.1
      29.0     100.0
      30.0       2.3
      31.0       3.3
      32.0       1.1
      41.0       2.9
      43.0       2.5
      45.0       7.8
      55.0       3.1
      56.0       7.1
      57.0      13.5
      62.0      20.4
      63.0      58.3
      64.0       7.8
      65.0      18.7
      73.0       2.2
      77.0       1.5
      91.0      11.1
      93.0       3.6
      97.0       2.2
      99.0       1.3
     136.0       1.3

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₅ H₉ Cl O₂	0.04 ml : 0.5 ml CDCl₃
ethyl 2-chloropropionate

    Assign.     Shift(ppm)

      A             4.368
      B             4.242
      C             1.692
      D             1.312

     Hz     ppm     Int.

    403.63   4.507     64
    396.56   4.428    191
    390.38   4.359    113
    389.63   4.351    209
    383.25   4.280    370
    376.13   4.200    399
    369.06   4.121    125
    154.88   1.730   1000
    152.56   1.704     30
    147.94   1.652    935
    124.31   1.389    406
    122.56   1.369     44
    117.31   1.310    923
    110.06   1.229    355

CCl4 solution

liquid film

4880 A,200 M,liquid

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