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MassMS-NW-3130 3-ethyl-4-methylpyridine C8H11N (Mass of molecular ion: 121)
Source Temperature: 280 °C Sample Temperature: 180 °C Reservoir, 75 eV
27.0 5.3 38.0 1.9 39.0 10.3 40.0 1.5 41.0 3.0 50.0 3.1 51.0 6.8 52.0 4.0 53.0 6.1 54.0 1.4 62.0 1.0 63.0 3.1 64.0 1.3 65.0 5.3 66.0 2.7 77.0 14.8 78.0 4.8 79.0 17.4 80.0 2.5 91.0 3.2 92.0 2.8 93.0 7.1 94.0 1.6 104.0 1.7 105.0 1.0 106.0 100.0 107.0 8.4 118.0 1.9 120.0 25.6 121.0 71.9 122.0 6.8
90 MHz in CDCl3
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1H NMR 89.56 MHz C8 H11 N 0.05 ml : 0.5 ml CDCl3 3-ethyl-4-methylpyridine 
Assign. Shift(ppm)
A 8.32 B 8.30 C 7.010 D 2.619 E 2.281 F 1.210
Hz ppm Int.746.31 8.334 280 740.19 8.265 190 630.25 7.038 138 625.31 6.983 127 246.19 2.749 63 238.63 2.665 214 233.81 2.611 32 231.00 2.580 239 228.56 2.553 29 223.56 2.497 97 204.31 2.282 1000 115.38 1.289 391 108.00 1.206 755 100.31 1.121 296
in CDCl3
liquid film
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