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MassMS-KW-0244 3-ethylpyridine C7H9N (Mass of molecular ion: 107)
Source Temperature: 230 °C Sample Temperature: 150 °C Reservoir, 75 eV
26.0 1.7 27.0 6.4 28.0 3.0 37.0 1.5 38.0 3.9 39.0 18.7 40.0 1.6 41.0 2.2 50.0 6.7 51.0 12.7 52.0 8.2 52.5 1.1 53.0 4.9 54.0 1.3 62.0 1.3 63.0 4.6 64.0 2.6 65.0 34.5 66.0 3.2 74.0 1.0 75.0 1.1 76.0 1.0 77.0 8.8 78.0 7.4 79.0 18.0 80.0 4.2 92.0 100.0 93.0 7.0 104.0 2.1 105.0 1.1 106.0 45.9 107.0 81.3 108.0 7.0
400 MHz in CDCl3
90 MHz in CDCl3
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1H NMR 399.65 MHz C7H9N 0.05 ml : 0.5 ml CDCl3 3-ethylpyridine 
Assign. Shift(ppm)
A 8.459 B 8.423 C 7.475 D 7.174 E 2.623 F 1.232
Hz ppm Int.3382.57 8.462 192 3380.86 8.457 191 3370.24 8.431 136 3368.78 8.427 142 3365.48 8.419 140 3363.90 8.415 141 2994.51 7.491 87 2992.80 7.487 127 2992.19 7.485 126 2990.48 7.481 89 2986.70 7.471 99 2984.99 7.467 140 2984.38 7.465 141 2982.67 7.461 97 2874.39 7.190 124 2873.66 7.189 127 2869.51 7.178 125 2868.78 7.176 127 2866.58 7.171 114 2865.85 7.169 116 2861.82 7.159 107 2861.09 7.157 110 1059.82 2.651 118 1052.25 2.633 320 1044.56 2.613 325 1036.87 2.594 126 555.06 1.389 9 500.13 1.251 625 492.44 1.232 1000 484.75 1.213 598 428.23 1.072 11
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1H NMR 89.56 MHz C7 H9 N 0.05 ml : 0.5 ml CDCl3 3-ethylpyridine Assign. Shift(ppm)
A 8.44 B 8.41 C 7.46 D 7.16 E 2.617 F 1.236
Hz ppm Int.756.31 8.445 302 751.75 8.394 154 750.13 8.376 145 674.88 7.536 66 673.06 7.516 95 672.50 7.509 87 671.88 7.503 58 671.44 7.498 56 670.81 7.491 64 667.06 7.449 116 666.38 7.441 101 665.31 7.429 161 664.75 7.423 148 663.63 7.410 88 663.00 7.403 99 647.00 7.225 145 646.38 7.218 130 644.75 7.200 30 644.25 7.194 30 642.31 7.172 135 641.50 7.163 123 639.25 7.138 94 638.56 7.130 82 634.56 7.086 82 633.88 7.078 72 633.75 7.077 72 246.69 2.755 84 239.25 2.672 265 236.31 2.639 37 231.63 2.587 299 224.06 2.502 118 117.94 1.317 488 110.56 1.235 1000 106.19 1.186 43 102.81 1.148 367
in CDCl3
liquid film
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