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2,4-DINITROBENZENESULFENYL CHLORIDE

Product Name 2,4-DINITROBENZENESULFENYL CHLORIDE

CAS528-76-7

MFC6H3ClN2O4S

MW234.62

¹³CNMR

400 MHz in DMSO-d6

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₆ H₃ Cl N₂ O₄ S	saturated in DMSO-d₆
2,4-dinitrobenzenesulfenyl chloride

    Assign.     Shift(ppm)

      A             8.566
      B             8.413
      C             8.099

     Hz     ppm     Int.

   3426.67   8.575     52
   3424.22   8.569    901
   3422.24   8.564   1000
   3367.92   8.428    688
   3365.63   8.422    612
   3361.82   8.412     34
   3359.38   8.406    740
   3357.09   8.401    667
   3239.29   8.106    986
   3233.80   8.092     31
   3230.74   8.084    826

¹H NMR	89.56 MHz
C₆ H₃ Cl N₂ O₄ S	0.048 g : 0.5 ml CDCl₃
2,4-dinitrobenzenesulfenyl chloride

    Assign.     Shift(ppm)

      A             9.155
      B             8.594
      C             8.243

     Hz     ppm     Int.

    823.38   9.194     41
    821.13   9.169    736
    818.81   9.143    818
    787.13   8.789     30
    778.31   8.691     30
    776.38   8.669    432
    774.06   8.643    376
    771.94   8.620     35
    770.69   8.606     30
    769.38   8.591     41
    767.31   8.568    668
    764.94   8.542    635
    744.63   8.315     28
    741.69   8.282   1000
    738.19   8.243     31
    737.69   8.237     36
    737.38   8.234     36
    732.56   8.180    602

in CDCl3

KBr disc

nujol mull

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